公开(公告)号：US09079777B2

公开(公告)日：2015-07-14

申请号：US14533560

申请日：2014-11-05

申请人： TOKUYAMA CORPORATION

发明人： Takayuki Maehara ,  Tadaharu Komatsubara ,  Yuya Yamano ,  Kenichi Ishizu ,  Makoto Sato ,  Hiroaki Taira ,  Hiroshi Kato

IPC分类号： C07F7/02 ,  C01B33/146 ,  C01B13/36 ,  C01B33/18 ,  C01B33/148 ,  C01G23/04 ,  C01G25/02 ,  C07F7/08 ,  C07F7/10

CPC分类号： C01B33/146 ,  C01B13/36 ,  C01B13/363 ,  C01B33/141 ,  C01B33/148 ,  C01B33/154 ,  C01B33/18 ,  C01G23/04 ,  C01G25/02 ,  C01P2004/52 ,  C01P2004/62 ,  C01P2004/64 ,  C07F7/08 ,  C07F7/10 ,  C09C1/3081

摘要： The present invention relates to a method for producing inorganic oxide particles, comprising at least the following steps of: coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst; filtering the dispersion to obtain particles; and drying the particles, wherein the step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion. The inorganic oxide particles obtained by the method of the present invention have high purity and are excellent in flowability.

摘要翻译： 本发明涉及无机氧化物粒子的制造方法，至少包括以下步骤：在碱性催化剂的存在下使通过进行水解反应和金属醇盐的缩聚反应得到的分散体凝结; 过滤分散体以获得颗粒; 并干燥所述颗粒，其中通过将至少一种选自二氧化碳，碳酸铵，碳酸氢铵和氨基甲酸铵的化合物的凝结剂加入到分散体中来进行凝固分散体的步骤。 通过本发明的方法获得的无机氧化物颗粒具有高纯度并且流动性优异。

公开(公告)号：US11254821B2

公开(公告)日：2022-02-22

申请号：US16495191

申请日：2018-03-27

申请人： TOKUYAMA CORPORATION

发明人： Takayuki Maehara ,  Qingtao Zhou ,  Jianzhang Dai

IPC分类号： B32B5/16 ,  B05D7/00 ,  C09C1/30 ,  C08G59/40 ,  C08G59/50 ,  C09J11/06 ,  C09J163/00

摘要： A silicone oil-treated fumed silica and a method of producing the silicone oil-treated fumed silica are provided. The silicone oil-treated fumed silica, which has the following physical properties: A) the silicone oil-treated fumed silica has a degree of hydrophobicity of 68 vol % or more; B) the silicone oil-treated fumed silica has a silicone oil fixation rate of from 60 mass % to 95 mass %; and C) a composition obtained by adding 6 parts by mass of the silicone oil-treated fumed silica to 100 parts by mass of an amine composition containing trimethylolpropane polyoxypropylene triamine and 1,3-bis(aminomethyl)cyclohexane at a mass ratio of 95:5 has a viscosity of 4,000 mPa·s or more after the composition is left to stand at 25° C. for 1 hour.