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公开(公告)号：US5912082A
公开(公告)日：1999-06-15
申请号：US638859
申请日：1996-04-29
IPC分类号： B32B17/10 , B32B27/30 , C03C27/12 , C08F214/06 , C08F214/14
CPC分类号： B32B17/1055 , C08F214/06 , Y10T428/31645
摘要： A process for polymerizing vinyl chloride alone or a mixture of vinyl chloride and other vinyl monomer(s) with hydroxy containing monomer(s), and the copolymer obtained thereby. The hydroxy containing monomer(s) is obtained by the partial allylation of dihydroxy or polyhydroxy alcohols. The copolymers are prepared by suspension polymerization. The presence of the hydroxyl groups significantly modifies the characteristics of the polymers. Plasticizer-take-up is increased and dry-time is reduced significantly. Furthermore, the hydroxyl groups become the sites for postpolymerization reactions due to their polarity and reactivity.
摘要翻译： 将氯乙烯单独聚合或氯乙烯和其它乙烯基单体与含羟基单体的混合物的方法和由此得到的共聚物。 含羟基的单体通过二羟基或多羟基醇的部分烯丙基化获得。 通过悬浮聚合制备共聚物。 羟基的存在显着地改变了聚合物的特性。 增塑剂吸收量增加，干燥时间显着降低。 此外，由于其极性和反应性，羟基成为后聚合反应的位点。
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公开(公告)号：US5863656A
公开(公告)日：1999-01-26
申请号：US56249
申请日：1998-04-07
CPC分类号： B32B17/1055 , B32B15/08 , B32B17/10036 , B32B17/10688 , B32B17/10715 , B32B17/10761 , B32B17/10779 , B32B27/10 , C08F214/06 , Y10T428/31518 , Y10T428/31645
摘要： An improved method is provided for copolymerizing vinyl chloride with allyl glycidyl ether and a vinyl ester. The copolymers so formed include 70-99 weight percent of vinyl chloride, 0.05-15 weight percent of allyl glycidyl ether, and 0.05-15 weight percent of a vinyl ester, preferably vinyl acetate. The copolymers of this invention can be compounded to provide films exhibiting improved heat stability, low haze, and good adhesion to solid surfaces such as glass and metal. The compounded resins thus obtained may be especially advantageously used in forming the interlayer of laminated safety glazings, such as vehicle windshields and architectural glazings.The copolymerization of vinyl chloride, allyl glycidyl ether, a vinyl ester and small amounts of an unsaturated organic trifunctional silane provide self-adhesion without gelation.
摘要翻译： 提供了一种用于使氯乙烯与烯丙基缩水甘油醚和乙烯基酯共聚的改进方法。 如此形成的共聚物包括70-99重量％的氯乙烯，0.05-15重量％的烯丙基缩水甘油醚和0.05-15重量％的乙烯基酯，优选乙酸乙烯酯。 可以将本发明的共聚物配混以提供具有改善的热稳定性，低雾度和对诸如玻璃和金属的固体表面的良好粘附性的膜。 由此获得的复合树脂可以特别有利地用于形成层压安全玻璃的中间层，例如车辆挡风玻璃和建筑玻璃。 氯乙烯，烯丙基缩水甘油醚，乙烯基酯和少量不饱和有机三官能硅烷的共聚合可提供自粘而无凝胶化。
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3.发明授权Laminated glazing unit comprising copolymers of vinyl chloride, allyl glycidyl ether, and a vinyl ester and method of making the same 失效包括氯乙烯，烯丙基缩水甘油醚和乙烯基酯的共聚物的层压玻璃单元及其制备方法
公开(公告)号：US5858542A
公开(公告)日：1999-01-12
申请号：US821510
申请日：1997-03-21
IPC分类号： C08F2/18 , B32B15/08 , B32B17/10 , B32B27/10 , C08F214/06
CPC分类号： B32B15/08 , B32B17/10036 , B32B17/1055 , B32B17/10688 , B32B17/10715 , B32B17/10761 , B32B17/10779 , B32B27/10 , C08F214/06 , Y10T428/31645 , Y10T428/31649
摘要： An improved method is provided for copolymerizing vinyl chloride with allyl glycidyl ether and a vinyl ester. The copolymers so formed include 70-99 weight % of vinyl chloride, 0.05-15 weight % of allyl glycidyl ether, and 0.05-15 weight % of a vinyl ester, preferably vinyl acetate. The copolymers of this invention can be compounded to provide films exhibiting improved heat stability, low haze, and good adhesion to solid surfaces such as glass and metal. The compounded resins thus obtained may be especially advantageously used in forming the interlayer of laminated safety glazings, such as vehicle windshields and architectural glazings.
摘要翻译： 提供了一种用于使氯乙烯与烯丙基缩水甘油醚和乙烯基酯共聚的改进方法。 如此形成的共聚物包括70-99重量％的氯乙烯，0.05-15重量％的烯丙基缩水甘油醚和0.05-15重量％的乙烯基酯，优选乙酸乙烯酯。 可以将本发明的共聚物配混以提供具有改善的热稳定性，低雾度和对诸如玻璃和金属的固体表面的良好粘附性的膜。 由此获得的复合树脂可以特别有利地用于形成层压安全玻璃的中间层，例如车辆挡风玻璃和建筑玻璃。
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4.发明授权Method for the suspension polymerization of a vinyl chloride/allyl ether copolymer 失效氯乙烯/烯丙基醚共聚物的悬浮聚合方法
公开(公告)号：US5756617A
公开(公告)日：1998-05-26
申请号：US713893
申请日：1996-09-17
IPC分类号： C08F2/20 , C08F14/06 , C08F214/06
CPC分类号： C08F214/06 , C08F14/06
摘要： A process for polymerizing vinyl chloride alone or a mixture of vinyl chloride and other vinyl monomer(s) with hydroxy containing monomer(s), and the copolymer obtained thereby. The hydroxy containing monomer(s) is obtained by the partial allylation of dihydroxy or polyhydroxy alcohols. The copolymers are prepared by suspension polymerization. The presence of the hydroxyl groups significantly modifies the characteristics of the polymers. Plasticizer-take-up is increased and dry-time is reduced significantly. Furthermore, the hydroxyl groups become the sites for postpolymerization reactions due to their polarity and reactivity.
摘要翻译： 将氯乙烯单独聚合或氯乙烯和其它乙烯基单体与含羟基单体的混合物的方法和由此得到的共聚物。 含羟基的单体通过二羟基或多羟基醇的部分烯丙基化获得。 通过悬浮聚合制备共聚物。 羟基的存在显着地改变了聚合物的特性。 增塑剂吸收量增加，干燥时间显着降低。 此外，由于其极性和反应性，羟基成为后聚合反应的位点。
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5.发明授权Copolymers of vinyl chloride, allyl glycidyl ether, a vinyl ester and an unsaturated organic trifunctional silane and method of making the same 失效氯乙烯，烯丙基缩水甘油醚，乙烯基酯和不饱和有机三官能硅烷的共聚物及其制备方法
公开(公告)号：US5747617A
公开(公告)日：1998-05-05
申请号：US726378
申请日：1996-10-04
IPC分类号： C08F2/18 , B32B15/08 , B32B17/10 , B32B27/10 , C08F214/06 , C08F224/00 , C08F216/12 , C08F218/08
CPC分类号： B32B17/1055 , B32B15/08 , B32B17/10036 , B32B17/10688 , B32B17/10715 , B32B17/10761 , B32B17/10779 , B32B27/10 , C08F214/06 , Y10T428/31518 , Y10T428/31645
摘要： An improved method is provided for copolymerizing vinyl chloride with allyl glycidyl ether and a vinyl ester. The copolymers so formed include 70-99 weight percent of vinyl chloride, 0.05-15 weight percent of allyl glycidyl ether, and 0.05-15 weight percent of a vinyl ester, preferably vinyl acetate. The copolymers of this invention can be compounded to provide films exhibiting improved heat stability, low haze, and good adhesion to solid surfaces such as glass and metal. The compounded resins thus obtained may be especially advantageously used in forming the interlayer of laminated safety glazings, such as vehicle windshields and architectural glazings. The copolymerization of vinyl chloride, allyl glycidyl ether, a vinyl ester and small amounts of an unsaturated organic trifunctional silane provide self-adhesion without gelation.
摘要翻译： 提供了一种用于使氯乙烯与烯丙基缩水甘油醚和乙烯基酯共聚的改进方法。 如此形成的共聚物包括70-99重量％的氯乙烯，0.05-15重量％的烯丙基缩水甘油醚和0.05-15重量％的乙烯基酯，优选乙酸乙烯酯。 可以将本发明的共聚物配混以提供具有改善的热稳定性，低雾度和对诸如玻璃和金属的固体表面的良好粘附性的膜。 由此获得的复合树脂可以特别有利地用于形成层压安全玻璃的中间层，例如车辆挡风玻璃和建筑玻璃。 氯乙烯，烯丙基缩水甘油醚，乙烯基酯和少量不饱和有机三官能硅烷的共聚合可提供自粘而无凝胶化。
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6.发明授权Copolymers of vinyl chloride, allyl glycidyl ether, and a vinyl ester and method of making the same 失效氯乙烯，烯丙基缩水甘油醚和乙烯基酯的共聚物及其制备方法
公开(公告)号：US5641845A
公开(公告)日：1997-06-24
申请号：US513693
申请日：1995-08-11
IPC分类号： C08F2/18 , B32B15/08 , B32B17/10 , B32B27/10 , C08F214/06 , C08F224/00 , C08F216/12 , C08F218/08
CPC分类号： B32B15/08 , B32B17/10036 , B32B17/1055 , B32B17/10688 , B32B17/10715 , B32B17/10761 , B32B17/10779 , B32B27/10 , C08F214/06 , Y10T428/31645 , Y10T428/31649
摘要： An improved method is provided for copolymerizing vinyl chloride with allyl glycidyl ether and a vinyl ester. The copolymers so formed include 70-99 weight % of vinyl chloride, 0.05-15 weight % of allyl glycidyl ether, and 0.05-15 weight % of a vinyl ester, preferably vinyl acetate. The copolymers of this invention can be compounded to provide films exhibiting improved heat stability, low haze, and good adhesion to solid surfaces such as glass and metal. The compounded resins thus obtained may be especially advantageously used in forming the interlayer of laminated safety glazings, such as vehicle windshields and architectural glazings.
摘要翻译： 提供了一种用于使氯乙烯与烯丙基缩水甘油醚和乙烯基酯共聚的改进方法。 如此形成的共聚物包括70-99重量％的氯乙烯，0.05-15重量％的烯丙基缩水甘油醚和0.05-15重量％的乙烯基酯，优选乙酸乙烯酯。 可以将本发明的共聚物配混以提供具有改善的热稳定性，低雾度和对诸如玻璃和金属的固体表面的良好粘附性的膜。 由此获得的复合树脂可以特别有利地用于形成层压安全玻璃的中间层，例如车辆挡风玻璃和建筑玻璃。
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公开(公告)号：US5756626A
公开(公告)日：1998-05-26
申请号：US695208
申请日：1996-08-07
IPC分类号： C08F14/06 , C08F116/18
CPC分类号： C08F14/06
摘要： A process for polymerizing vinyl chloride alone or a mixture of vinyl chloride and other vinyl monomer(s) with hydroxy containing monomer(s), and the copolymer obtained thereby. The hydroxy containing monomer(s) is obtained by the partial allylation of dihydroxy or polyhydroxy alcohols. The copolymers are prepared by suspension polymerization. The presence of the hydroxyl groups significantly modifies the characteristics of the polymers. Plasticizer-take-up is increased and dry-time is reduced significantly. Furthermore, the hydroxyl groups become the sites for postpolymerization reactions due to their polarity and reactivity.
摘要翻译： 将氯乙烯单独聚合或氯乙烯和其它乙烯基单体与含羟基单体的混合物的方法和由此得到的共聚物。 含羟基的单体通过二羟基或多羟基醇的部分烯丙基化获得。 通过悬浮聚合制备共聚物。 羟基的存在显着地改变了聚合物的特性。 增塑剂吸收量增加，干燥时间显着降低。 此外，由于其极性和反应性，羟基成为后聚合反应的位点。
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公开(公告)号：US6001462A
公开(公告)日：1999-12-14
申请号：US611689
申请日：1996-03-06
IPC分类号： B32B7/02 , B32B7/14 , B32B9/00 , B32B17/10 , B32B27/06 , C03C17/28 , C03C17/30 , C03C27/12 , C08K3/24 , C08K3/28 , C08K3/32 , C08K5/00 , C08K5/07 , C08K5/09 , C08K5/098 , C08K5/10 , C08K5/1515 , C08L27/06
CPC分类号： C08K5/0008 , B32B17/10036 , B32B17/1055 , B32B17/10688 , B32B27/06 , C03C17/30 , C08K5/10 , Y10T428/24967 , Y10T428/266 , Y10T428/31649
摘要： A laminated safety glass is formed of an inboard glass sheet, an outboard glass sheet and a plasticized polyvinyl chloride containing interlayer therebetween. The outboard glass sheet has an average transmittance of radiation in the range of 300-340 nm of less than about 20%, and preferably less than about 1%. The outboard glass sheet also has an average transmittance of radiation in the range of 340 to 500 nm of more than about 50%. The outboard glass sheet may be formed of an ultraviolet radiation absorbing glass, such as an ultraviolet radiation absorbing green glass.
摘要翻译： 层压安全玻璃由内侧玻璃板，外侧玻璃板和含有中间层的塑化聚氯乙烯形成。 外侧玻璃板具有300-340nm范围内的辐射的平均透射率小于约20％，优选小于约1％。 外侧玻璃板还具有在340至500nm范围内的辐射的平均透射率大于约50％。 外侧玻璃板可以由紫外线吸收玻璃形成，例如紫外线吸收绿色玻璃。
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公开(公告)号：US5593786A
公开(公告)日：1997-01-14
申请号：US336477
申请日：1994-11-09
CPC分类号： B32B17/10036 , B32B17/10 , Y10T428/31612 , Y10T428/31645 , Y10T428/31649 , Y10T428/31909 , Y10T428/3192
摘要： Laminated safety glass includes a pair of glass sheets bonded together with a self-adhering composite interlayer. The composite interlayer is formed of a support layer including a plasticized PVC containing film and a polymeric adhesive layer on one, or preferably both, of the major surfaces of the support layer. The adhesive layers are formed of a polymeric material which is capable of adhering to the PVC containing support layer and to the glass sheets. The respective refractive indices of the adhesive layers and the support layer are matched as closely as possible in order to eliminate optical distortion caused by interfacial reflections of incident light. A preferred copolymer resin for forming the adhesive layers is poly(vinyl chloride-co-vinyl acetate-co-maleic acid).
摘要翻译： 层压安全玻璃包括一对与自粘复合中间层结合在一起的玻璃板。 复合中间层由支撑层形成，该支撑层包括增塑的含PVC膜和在支撑层的主表面的一个或优选两个上的聚合物粘合剂层。 粘合层由能够粘附到含PVC载体层和玻璃板上的聚合物材料形成。 为了消除由入射光的界面反射引起的光学变形，粘合剂层和支撑层的各自的折射率尽可能地匹配。 用于形成粘合剂层的优选共聚物树脂是聚（氯乙烯 - 共 - 乙酸乙烯酯 - 共 - 马来酸）。
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公开(公告)号：US20150122319A1
公开(公告)日：2015-05-07
申请号：US13261804
申请日：2011-07-28
申请人： David A. Strickler , Yu Wang , Jun Ni , Troy D. Manning
发明人： David A. Strickler , Yu Wang , Jun Ni , Troy D. Manning
IPC分类号： H01L31/0224 , H01L31/18
CPC分类号： H01L31/022425 , C03C17/2456 , C03C2217/212 , C03C2217/218 , C03C2217/24 , C03C2218/1525 , C23C16/405 , C23C16/46 , C23C16/545 , H01L31/022466 , H01L31/1884 , Y02E10/50
摘要： A method of making a doped titanium oxide coating in a float glass manufacturing process and the coated glass article made thereby wherein the dopant is a niobium or tantalum compound. The doped titanium oxide coating preferably exhibits an electrical conductivity >1×10−3 S/cm.
摘要翻译： 在浮法玻璃制造工艺中制造掺杂的氧化钛涂层的方法和由此制成的涂覆的玻璃制品，其中掺杂剂是铌或钽化合物。 掺杂的氧化钛涂层的电导率优选> 1×10 -3 S / cm。
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