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    Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same
    2.
    发明授权
    Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same 失效
    叔羟基醛，其感官用途及其制备方法

    公开(公告)号：US4554385A

    公开(公告)日：1985-11-19

    申请号：US709916

    申请日：1985-03-08

    申请人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    发明人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC分类号： C07C47/36 ,  C07C47/19

    CPC分类号： C07C47/36

    摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).

    摘要翻译： 描述的是根据通用结构定义的叔羟基醛：其中当m不为0时，线和 - - - - 和/或+ + + + +代表共价碳 - 碳键; 并且当m = 0时，线+ + + + +和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个用代表碳 - 碳键的+ + + + +和 - 当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z与所述线完成环烷基环部分，并且+ + + + +代表碳 - 碳键，并且具有不代表键的线 - - - - - 。 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在 增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜和 喜欢）。

    Ether carbinols and process for preparing same
    5.
    发明授权
    Ether carbinols and process for preparing same 失效
    醚甲醇及其制备方法

    公开(公告)号：US4521634A

    公开(公告)日：1985-06-04

    申请号：US574150

    申请日：1984-01-26

    申请人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    发明人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC分类号： A24B15/34 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C11B9/00 ,  C07C43/188 ,  C07C41/06

    CPC分类号： C11B9/0046 ,  A24B15/345 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C07C2102/42

    摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene or C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture of carbon monoxide and hydrogen by means of an oxoreaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.

    摘要翻译： 描述根据通用结构定义的醚甲醇：其中X 1表示选自下列的部分：其中Y 1表示C 4或C 5亚烷基或C 4或C 5亚链烯基或C 4或C 4 C5亚炔基; 通过首先使烯丙基醚与一氧化碳和氢气的混合物通过氧化反应制备这种醚甲醇的方法，以产生醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。 还描述了具有以下结构之一的两种醚甲醛：通过使一种合适的烯丙基醚与一氧化碳和氢气的混合物通过氧代反应制备这种醚甲醛的方法 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

    Polyhydroindan carboxaldehydes and uses thereof in augmenting or enhancing the aromas of perfume compositions, colognes and perfumed articles
    8.
    发明授权
    Polyhydroindan carboxaldehydes and uses thereof in augmenting or enhancing the aromas of perfume compositions, colognes and perfumed articles 失效

    公开(公告)号：US4622171A

    公开(公告)日：1986-11-11

    申请号：US712164

    申请日：1985-03-15

    申请人： Mark A. Sprecker ,  William L. Schreiber ,  Futoshi Fujioka ,  Richard M. Boden ,  Manfred H. Vock ,  Patrick Whelan ,  Marie R. Hanna

    发明人： Mark A. Sprecker ,  William L. Schreiber ,  Futoshi Fujioka ,  Richard M. Boden ,  Manfred H. Vock ,  Patrick Whelan ,  Marie R. Hanna

    IPC分类号： C07C45/49 ,  C07C45/50 ,  C07C47/36 ,  C07C47/37 ,  C07C47/445 ,  C07C49/523 ,  C11B9/00 ,  A61K7/46

    CPC分类号： C11B9/0042 ,  C07C45/49 ,  C07C45/50 ,  C07C47/36 ,  C07C47/37 ,  C07C47/445 ,  C07C49/523

    摘要： Described is the genus of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein each of the dashed lines represent carbon-carbon single bonds or carbon-carbon double bonds with the proviso that at least one of the dashed lines represents a carbon-carbon single bond; wherein one of R.sub.1, R.sub.2 and R.sub.3 is hydrogen or methyl and each of the other of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; wherein one of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen or methyl and each of the other of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen; wherein m is 0 or 1 and n is 0 or 1 and the sum of m+n=1; wherein X' represents one of the moieties: ##STR2## wherein R.sub.7 represents C.sub.1 -C.sub.3 alkyl or acetyl; and wherein R.sub.8 represents C.sub.1 -C.sub.3 alkyl, with the proviso that when X' is methylene having the structure: ##STR3## then m is 0 and n is 1 and with the further proviso that when n is 0, one of the dashed lines is a carbon-carbon double bond; and one of R.sub.1, R.sub.2 and R.sub.3 represents methyl and one of R.sub.4, R.sub.5, and R.sub.6 represents methyl, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, perfumed polymers and cosmetic powders). Also described is a process for preparing such polyhydroindan carboxaldehydes by reacting a tricyclic compound or mixture of compounds defined according to the structure: ##STR4## with carbon monoxide and hydrogen via an "oxo" reaction; wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are defined, supra; wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein X" represents one of the moieties: with the proviso that when X' is methylene having the structure: ##STR5## then the line:+++++is a double bond and when X' is not methylene having the structure: ##STR6## then the line:+++++is a carbon-carbon single bond.

    Ether carbinols
    9.
    发明授权
    Ether carbinols 失效
    乙醚甲醇

    公开(公告)号：US4620041A

    公开(公告)日：1986-10-28

    申请号：US784618

    申请日：1985-10-04

    申请人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    发明人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC分类号： A24B15/34 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C11B9/00

    CPC分类号： C11B9/0046 ,  A24B15/345 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C07C2102/42

    摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene; C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture or carbon monoxide and hydrogen by means of an oxo reaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colgnes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.

    摘要翻译： 描述了根据通用结构定义的醚甲醇：其中X 1表示选自以下的部分：其中Y 1表示C 4或C 5亚烷基; C4或C5亚链烯基或C4或C5亚炔基; 通过首先使烯丙基醚与混合物或一氧化碳和氢气通过羰基反应反应生成醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇来制备此类醚甲醇的方法; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。 还描述了具有以下结构之一的两个醚甲醛：＆lt; IMAGE＆gt;和＆lt; IMAGE＆gt;用于通过使羰基合成的烯丙基醚与一氧化碳和氢的混合物通过氧代 - 以及用于增强或增强消耗材料的香气或味道的方法，包括香料，水泥和香料制品; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

    Preparing a tertiary hydroxyl carboxaldehyde containing perfume composition
    10.
    发明授权
    Preparing a tertiary hydroxyl carboxaldehyde containing perfume composition 失效
    制备含羟基甲醛的香料组合物

    公开(公告)号：US4608195A

    公开(公告)日：1986-08-26

    申请号：US768839

    申请日：1985-08-23

    申请人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    发明人： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC分类号： C07C45/49 ,  C07C47/27 ,  C07C47/36 ,  C11B9/00 ,  A61K7/46

    CPC分类号： C11B9/0061 ,  C07C45/49 ,  C07C47/27 ,  C07C47/36

    摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).

    摘要翻译： 描述的是根据通用结构定义的叔羟基甲醛：其中当m不为0时，线* * * * *和 - - - - - 和/或+ + + + +代表共价碳 - 碳键 ; 并且当m = 0时，线+ + + + + * * * * *和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个完成具有代表碳 - 碳键的线+ + + + + * * * * *和 - - - - 的双环的所需的碳原子。 当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z完全是环烷基环部分，其中线* * * *和+ + + +代表碳 - 碳键，并且线 - - - - - 不表示键; 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在 增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜等）的香气 ）。