Method for preparing ammonium hydroxyalkyl sulfonates and ammonium
alkanoyl alkyl sulfonates produced therefrom
    1.
    发明授权
    Method for preparing ammonium hydroxyalkyl sulfonates and ammonium alkanoyl alkyl sulfonates produced therefrom 失效
    制备羟基烷基磺酸铵和烷基磺酸烷基磺酸铵的方法

    公开(公告)号:US5739365A

    公开(公告)日:1998-04-14

    申请号:US509018

    申请日:1995-07-28

    IPC分类号: C07C303/02 C07C53/00

    CPC分类号: C07C303/02

    摘要: A method is disclosed for preparing ammonium hydroxyalkyl sulfonate by a process of reacting ammonium bisulfite and alkylene oxide wherein the pH is maintained at a relatively low value throughout most of the time of reaction of ammonium bisulfite and alkylene oxide in order to minimize the quantity of impurities, e.g. alkylene glycol and alkanolamine, in the ammonium hydroxyalkyl sulfonate. Ammonium alkanoyl alkyl sulfonates prepared by reacting such ammonium hydroxyalkyl sulfonates with fatty acids form aqueous solutions which are clear at ambient temperatures, and thus are useful as surfactants in clear liquid products.

    摘要翻译: 公开了通过使亚硫酸氢铵和烯化氧反应制备铵羟烷基磺酸铵的方法,其中在亚硫酸氢铵和环氧烷反应的大部分时间内将pH保持在相对较低的值,以使杂质的量最小化 ,例如 烷基二醇和链烷醇胺,在羟烷基磺酸铵中。 通过使这种羟基烷基磺酸铵与脂肪酸反应制备的烷基磺酸烷基磺酸盐形成在环境温度下是透明的水溶液,因此可用作透明液体产物中的表面活性剂。

    N-hydroxysuccinimide monohydrate
    3.
    发明授权
    N-hydroxysuccinimide monohydrate 失效
    N-羟基琥珀酰亚胺一水合物

    公开(公告)号:US5493031A

    公开(公告)日:1996-02-20

    申请号:US260637

    申请日:1994-06-16

    IPC分类号: C07D207/46

    CPC分类号: C07D207/46

    摘要: N-hydroxysuccinimide monohydrate is precipitated from an aqueous solution of N-hydroxysuccinimide. N-hydroxysuccinimide monohydrate is a new compound that can be used to produce anhydrous N-hydroxysuccinimide which is substantially pure. It can also be used as a substitute for N-hydroxysuccinimide when the presence of water is not detrimental.

    摘要翻译: N-羟基琥珀酰亚胺一水合物从N-羟基琥珀酰亚胺的水溶液中沉淀出来。 N-羟基琥珀酰亚胺一水合物是可用于制备基本上纯的无水N-羟基琥珀酰亚胺的新化合物。 当水的存在不是有害的时,它也可以用作N-羟基琥珀酰亚胺的替代物。

    Soil release composition for use with polyester textiles
    6.
    发明授权
    Soil release composition for use with polyester textiles 失效
    用于聚酯纺织品的土壤释放组合物

    公开(公告)号:US5370933A

    公开(公告)日:1994-12-06

    申请号:US830044

    申请日:1992-01-31

    摘要: Disclosed is a soil release composition for application to or finishing on polyester textile that is heat set at a temperature of 375.degree. F. (191.degree. C.) or higher, said composition comprising a non-fiber forming polyester-polyether copolymer and an antioxidantly effective amount of an acid catalyzed phenol-formaldehyde condensation product of the Novolak type.

    摘要翻译: 公开了一种在375°F(191℃)或更高温度下热定型的聚酯纺织品的涂布或整理剂的去污组合物,所述组合物包含非纤维形成聚酯 - 聚醚共聚物和抗氧化剂 有效量的酚醛清漆型酸催化酚醛缩合产物。

    Toluene sulfonate salts of 2-alkyl imidazolines
    8.
    发明授权
    Toluene sulfonate salts of 2-alkyl imidazolines 失效
    2-烷基咪唑啉的甲苯磺酸盐

    公开(公告)号:US4973616A

    公开(公告)日:1990-11-27

    申请号:US485189

    申请日:1990-02-26

    摘要: Toluene sulfonate salts of 2-alkyl imidazolines, e.g., 2-undecyl-4,4,5,5-tetramethyl imidazoline, are described. These compounds may be used as internal or external antistatic agents for fibers, e.g., acrylic fibers, and synthetic polymers, e.g., polystyrene.

    摘要翻译: 描述2-烷基咪唑啉的甲苯磺酸盐,例如2-十一烷基-4,4,5,5-四甲基咪唑啉。 这些化合物可以用作纤维的内部或外部抗静电剂,例如丙烯酸纤维,以及合成聚合物,例如聚苯乙烯。

    Method for preparing amino acid esters of nucleoside analogues
    9.
    发明申请
    Method for preparing amino acid esters of nucleoside analogues 审中-公开
    制备核苷类似物氨基酸酯的方法

    公开(公告)号:US20060178512A1

    公开(公告)日:2006-08-10

    申请号:US11051895

    申请日:2005-02-04

    IPC分类号: C07F9/6512

    CPC分类号: C07D473/00

    摘要: Describes a process for preparing esters of nucleoside analogues comprising condensing a nucleoside analogue with a protected amino acid in the presence of a tertiary amine and in the presence of an activating amount of an activating agent chosen from organo phosphoryl halide, organo phosphinic halide, aliphatic sulfonyl halide, and aromatic sulfonyl halide.

    摘要翻译: 描述了制备核苷类似物的酯的方法,包括在叔胺存在下将核苷类似物与受保护的氨基酸缩合,并且在活化剂量的活化剂存在下,选自有机磷酰卤,有机次膦酰卤,脂族磺酰基 卤化物和芳族磺酰卤。

    Method of preparing N-1-alkenyl carbonylamino compounds
    10.
    发明授权
    Method of preparing N-1-alkenyl carbonylamino compounds 失效
    制备N-1-链烯基羰基氨基化合物的方法

    公开(公告)号:US6140531A

    公开(公告)日:2000-10-31

    申请号:US280193

    申请日:1999-03-29

    CPC分类号: C07C269/00

    摘要: Describes a method of producing N-1-alkenyl carbonylamino compounds represented by the following general formula I, ##STR1## wherein R.sub.1 is the residue of an active hydrogen functional material, n is a number from 1 to a number equal to the number of active hydrogen groups of said active hydrogen functional material, X is selected from O, S and N(R.sub.5), R.sub.5 being hydrogen, hydrocarbyl, or R.sub.5 and R.sub.1 may together form a cyclic ring, R.sub.2, R.sub.3 and R.sub.4 are each independently selected from hydrogen, C.sub.1 -C.sub.4 alkyl and C.sub.2 -C.sub.4 alkenyl. The method comprises the steps of: (a) heating 2-alkenoyl azide in the presence of a first inert solvent in a first reaction zone, the first inert solvent being substantially free of active hydrogen functional material; (b) transferring volatile product as it is formed in the first reaction zone of step (a) into a separate second reaction zone containing a reactive composition comprising active hydrogen functional material having active hydrogen groups selected from the group consisting of hydroxyl, thiol, primary amine, secondary amine and combinations thereof; and (c) withdrawing N-1-alkenyl carbonylamino compound from the second reaction zone.

    摘要翻译: 描述了由以下通式I表示的制备N-1-链烯基羰基氨基化合物的方法,其中R 1是活性氢官能材料的残基,n是1至等于活性氢基团数目的数 所述活性氢官能材料,X选自O,S和N(R 5),R 5是氢,烃基或R 5,R 1可以一起形成环,R 2,R 3和R 4各自独立地选自氢,C1- C4烷基和C2-C4烯基。 该方法包括以下步骤:(a)在第一反应区中在第一惰性溶剂存在下加热2-烯酰基叠氮化物,第一惰性溶剂基本上不含活性氢官能材料; (b)将在步骤(a)的第一反应区中形成的挥发性产物转移到单独的第二反应区中,所述第二反应区含有包含活性氢官能团的反应性组合物,所述活性氢官能材料具有选自羟基,硫醇,伯 胺,仲胺及其组合; 和(c)从第二反应区取出N-1-链烯基羰基氨基化合物。