公开(公告)号：US09376370B2

公开(公告)日：2016-06-28

申请号：US14437172

申请日：2013-10-22

Applicant: CJ CHEILJEDANG CORP.

Inventor： Won Sik Gwak ,  Yong Bum Seo ,  Chong Ho Lee ,  In Sung Lee ,  Hideki Murata

IPC: C07C209/84 ,  C07C211/09 ,  C08G69/26 ,  C12P13/00

CPC classification number: C07C209/84 ,  C07C211/09 ,  C08G69/26 ,  C12P13/001

Abstract: A purification method of 1,4-diaminobutane, 1,4-diaminobutane purified using the purification method, and a polyamide prepared using the purified 1,4-diaminobutane are provided. The purification method of 1,4-diaminobutane includes: concentrating a fermentation solution including at least one of 1,4-diaminobutane and a salt thereof to obtain a concentrate; adding a base to the concentrate of the fermentation solution to prepare an basic composition having a pH 12 or higher; and recovering 1,4-diaminobutane from the basic composition.

Abstract translation: 提供使用纯化方法纯化的1,4-二氨基丁烷，1,4-二氨基丁烷的纯化方法和使用纯化的1,4-二氨基丁烷制备的聚酰胺。 1,4-二氨基丁烷的纯化方法包括：浓缩包含1,4-二氨基丁烷及其盐中的至少一种的发酵溶液以获得浓缩物; 向发酵溶液的浓缩物中加入碱以制备pH12或更高的碱性组合物; 并从碱性组合物中回收1,4-二氨基丁烷。

公开(公告)号：US09963421B2

公开(公告)日：2018-05-08

申请号：US14767814

申请日：2015-03-19

Applicant: CJ CHEILJEDANG CORP.

Inventor： Won Sik Gwak ,  Hyun Ju Won ,  Hideki Murata ,  Chong Ho Lee

IPC: C07C209/84 ,  C07C211/09 ,  C12P13/00

CPC classification number: C07C209/84 ,  C07C211/09 ,  C12P13/001

Abstract: Provided are a method of refining a reaction solution including a carbonate of 1,5-diaminopentane, which is produced by fermentation, through a decarbonation step and a pH adjustment step, and 1,5-diaminopentane which is refined by the above method.

公开(公告)号：US20150284315A1

公开(公告)日：2015-10-08

申请号：US14437172

申请日：2013-10-22

Applicant: CJ CHEILJEDANG CORP.

Inventor： Won Sik Gwak ,  Yong Bum Seo ,  Chong Ho Lee ,  In Sung Lee ,  Hideki Murata

IPC: C07C209/84 ,  C07C211/09

CPC classification number: C07C209/84 ,  C07C211/09 ,  C08G69/26 ,  C12P13/001

Abstract: A purification method of 1,4-diaminobutane, 1,4-diaminobutane purified using the purification method, and a polyamide prepared using the purified 1,4-diaminobutane are provided. The purification method of 1,4-diaminobutane includes: concentrating a fermentation solution including at least one of 1,4-diaminobutane and a salt thereof to obtain a concentrate; adding a base to the concentrate of the fermentation solution to prepare an basic composition having a pH 12 or higher; and recovering 1,4-diaminobutane from the basic composition.

Abstract translation: 提供使用纯化方法纯化的1,4-二氨基丁烷，1,4-二氨基丁烷的纯化方法和使用纯化的1,4-二氨基丁烷制备的聚酰胺。 1,4-二氨基丁烷的纯化方法包括：浓缩包含1,4-二氨基丁烷及其盐中的至少一种的发酵溶液以获得浓缩物; 向发酵溶液的浓缩物中加入碱以制备pH12或更高的碱性组合物; 并从碱性组合物中回收1,4-二氨基丁烷。