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公开(公告)号：US20110089019A1
公开(公告)日：2011-04-21
申请号：US12935661
申请日：2009-03-18
IPC分类号： C07C231/00 , C07B45/00 , C07C233/65
CPC分类号： C07C231/02 , B01J19/126 , C07D213/82 , C07C233/65 , C07C235/60
摘要： The invention relates to a continuous method for producing amides of aromatic carboxylic acids, according to which at least one aromatic carboxylic acid of formula (I) Ar—COON (I) wherein Ar is an optionally substituted aryl radical comprising between 5 and 50 atoms, is reacted with at least one amine of formula (II) HNR1R2 (II) wherein R1 and R2 are independently hydrogen or a hydrocarbon radical comprising between 1 and 100 C atoms, to form an ammonium salt, and said ammonium salt is then reacted to form a carboxylic acid amide, under microwave irradiation in a reaction pipe, the longitudinal axis of the pipe being oriented in the direction of propagation of the microwaves of a monomode microwave applicator.
摘要翻译： 本发明涉及一种生产芳族羧酸酰胺的连续方法，根据该方法，至少一种式（I）Ar-COON（I）的芳族羧酸，其中Ar是包含5至50个原子的任选取代的芳基， 与式（II）HNR1R2（II）的至少一种胺反应，其中R 1和R 2独立地为氢或包含1至100个C原子的烃基，以形成铵盐，然后所述铵盐反应形成 羧酸酰胺，在反应管中的微波照射下，管的纵向轴线沿着单模微波施加器的微波的传播方向取向。
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公开(公告)号：US08884040B2
公开(公告)日：2014-11-11
申请号：US12935628
申请日：2009-03-18
IPC分类号： C07C231/00 , C07C231/02
CPC分类号： C07C231/02 , C07C233/05 , C07C233/09 , C07C233/36
摘要： The invention relates to a continuous method for producing fatty acid amides, according to which at least one fatty acid of formula (I), R3—COOH (I) wherein R3 is an optionally substituted aliphatic hydrocarbon radical, is reacted with at least one amine of formula (II), HNR1R2 (II) wherein R1 and R2 are independently hydrogen or a hydrocarbon radical comprising between 1 and 100 C atoms, to form an ammonium salt, and said ammonium salt is then reacted to form a fatty acid amide, under microwave irradiation in a reaction pipe, the longitudinal axis of the pipe being oriented in the direction of propagation of the microwaves of a monomode microwave applicator.
摘要翻译： 本发明涉及一种生产脂肪酸酰胺的连续方法，根据该方法，将至少一种式（I）的脂肪酸，其中R 3为任选取代的脂族烃基的R 3 -COOH（I）与至少一种胺 式（II）的HNR1R2（II），其中R1和R2独立地为氢或包含1至100个C原子的烃基，以形成铵盐，然后所述铵盐反应形成脂肪酸酰胺， 在反应管中的微波照射，管的纵向轴线沿着单模微波施加器的微波的传播方向取向。
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公开(公告)号：US20110092722A1
公开(公告)日：2011-04-21
申请号：US12935628
申请日：2009-03-18
IPC分类号： C07C233/01
CPC分类号： C07C231/02 , C07C233/05 , C07C233/09 , C07C233/36
摘要： The invention relates to a continuous method for producing fatty acid amides, according to which at least one fatty acid of formula (I), R3—COOH (I) wherein R3 is an optionally substituted aliphatic hydrocarbon radical, is reacted with at least one amine of formula (II), HNR1R2 (II) wherein R1 and R2 are independently hydrogen or a hydrocarbon radical comprising between 1 and 100 C atoms, to form an ammonium salt, and said ammonium salt is then reacted to form a fatty acid amide, under microwave irradiation in a reaction pipe, the longitudinal axis of the pipe being oriented in the direction of propagation of the microwaves of a monomode microwave applicator.
摘要翻译： 本发明涉及一种生产脂肪酸酰胺的连续方法，根据该方法，将至少一种式（I）的脂肪酸，其中R 3为任选取代的脂族烃基的R 3 -COOH（I）与至少一种胺 式（II）的HNR1R2（II），其中R1和R2独立地为氢或包含1至100个C原子的烃基，以形成铵盐，然后所述铵盐反应形成脂肪酸酰胺， 在反应管中的微波照射，管的纵向轴线沿着单模微波施加器的微波的传播方向取向。
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