摘要:
The invention is directed to a process for the preparation of a cyclic carbamate starting with o-aminobenzyl alcohol and/or a suitable salt thereof, which is reacted with a cyclisation agent selected from phosgene, diphosgene, triphosgene and mixtures thereof, and in that the reaction carried out in the presence of an aqueous base, and a water-immiscible organic solvent, said organic solvent mainly comprising at least one compound selected from C2-5-alkyl C2-5-carboxylates and mixtures of at least one C2-5-alkyl C2-5-carboxylate with at least one C5-8-alkane.
摘要:
Roll for smoothing a web and method of making the roll, wherein the roll includes a hard roll core. An elastic covering layer is arranged on an outside surface of the hard roll core. The elastic covering layer includes an elastic matrix material and fibers embedded in the elastic matrix material. At least some of the fibers have a diameter which is less than 800 nm. A surface of the elastic covering layer has an extremely high smoothness. The method includes introducing the fibers into the elastic matrix material to form the elastic covering layer and coupling the elastic covering layer with the hard roll core.
摘要:
Reel slitting device for a web that includes a web supply section, a longitudinal slitting section, and a reeling section, and method for packaging partial rolls in the reeling section of the roll slitting device. The device includes at least one propelling device for reeling at least one partial roll and a packaging device that packages at least a periphery of the at least one partial roll. The the packaging device utilizes the at least one propelling device. The method includes slitting a web sheet into a plurality of partial webs, reeling the partial webs, in the reeling section, into a plurality of partial rolls, attaching a packaging web to a peripheral portion of at least one of the plurality of partial rolls in the reeling section, and rotating the at least one of the plurality of partial rolls to wind the packaging web around a radial surface of the at least one of the plurality of partial rolls.
摘要:
The invention is directed to a process for the preparation of a cyclic carbamate starting with o-aminobenzyl alcohol and/or a suitable salt thereof, which is reacted with a cyclization agent selected from phosgene, diphosgene, triphosgene and mixtures thereof, and in that the reaction carried out in the presence of an aqueous base, and a water-immiscible organic solvent, said organic solvent mainly comprising at least one compound selected from C2-5-alkyl C2-5-carboxylates and mixtures of at least one C2-5-alkyl C2-5-carboxylate with at least one C5-8-alkane.
摘要:
A roll for smoothing a web, a process for making the roll and a process of repairing the roll. The roll includes a roll core having an outer surface. A covering layer is disposed on the outer surface of the roll core. The covering layer has an inner surface and an outer surface. The covering layer includes an elastic matrix material. The elastic matrix material includes a mixture of at least one thermosetting plastic and at least one thermoplastic. The process of making includes providing a roll core having an outer surface, forming an elastic covering layer including at least one thermosetting plastic and at least one thermoplastic, and applying the covering layer to the outer surface of the roll core. The process of repairing includes heating an elastic covering layer made from an elastic matrix material which comprises at least one thermosetting plastic and at least one thermoplastic, and allowing any markings in a surface of the covering layer to be filled.
摘要:
The invention is directed to a process for the preparation of a cyclic carbamate starting with a chiral propargylic alcohol and/or a suitable salt thereof, which is reacted with a cyclization agent selected from phosgene, diphosgene, triphosgene and mixtures thereof, and in that the reaction is carried out in the presence of an aqueous base, and a water-immiscible organic solvent, said organic solvent mainly comprising at least one compound selected from C2-5-alkyl C2-5-carboxylates and mixtures of at least one C2-5-alkyl C2-5-carboxylate with at least one C5-8-alkane. Another aspect of the invention is directed to a process for the synthesis of said cyclic carbamate starting described above, wherein also a process for the preparation of the chiral propargylic alcohol is provided.
摘要翻译:本发明涉及一种制备环状氨基甲酸酯的方法,其起始于手性炔丙醇和/或其合适的盐,其与选自光气,双光气,三光气及其混合物的环化剂反应, 反应在碱水溶液和水不混溶的有机溶剂的存在下进行,所述有机溶剂主要包含至少一种选自C 2-5 - C 2-8 - C 2-8 - 羧酸烷基酯的化合物和至少一种C2-5-羧酸盐的混合物 - 烷基C2-5-羧酸酯与至少一种C5-8-烷烃。 本发明的另一方面涉及一种合成上述环状氨基甲酸酯的方法,其中还提供了制备手性炔丙醇的方法。
摘要:
The invention is directed to a process for the preparation of a cyclic carbamate starting with a chiral propargylic alcohol and/or a suitable salt thereof, which is reacted with a cyclisation agent selected from phosgene, diphosgene, triphosgene and mixtures thereof, and in that the reaction is carried out in the presence of an aqueous base, and a water-immiscible organic solvent, said organic solvent mainly comprising at least one compound selected from C2-5-alkyl C2-5-carboxylates and mixtures of at least one C2-5-alkyl C2-5-carboxylate with at least one C5-8-alkane. Another aspect of the invention is directed to a process for the synthesis of said cyclic carbamate starting described above, wherein also a process for the preparation of the chiral propargylic alcohol is provided.
摘要翻译:本发明涉及一种由手性炔丙醇和/或其合适的盐开始制备环状氨基甲酸酯的方法,其与选自光气,双极光,三光气及其混合物的环化剂反应, 反应在碱水溶液和水不混溶的有机溶剂的存在下进行,所述有机溶剂主要包含至少一种选自C 2-5 - C 2-8 - C 2-8 - 羧酸烷基酯的化合物和至少一种C2-5-羧酸盐的混合物 - 烷基C2-5-羧酸酯与至少一种C5-8-烷烃。 本发明的另一方面涉及一种合成上述环状氨基甲酸酯的方法,其中还提供了制备手性炔丙醇的方法。
摘要:
Calender for the treatment of a paper web including a roll stack of at least three rolls and with least one double-soft nip. The double-soft nip(s) are formed by two rolls, each with an elastic surface layer. At least one of the rolls forming the double-soft nip is heated. In a process using the calendar to treat a material web, the web is introduced into a roll stack having at least two rolls formed with an elastic surface layer over a rigid core, agglomerated in an elastic double-soft nip between the two rolls, heated to introduce energy into the material web and promote agglomerating, and smoothed in the elastic double-soft nip.