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    Halide-based scintillator nanomaterial
    1.
    发明申请
    Halide-based scintillator nanomaterial 有权
    卤化物闪烁体纳米材料

    公开(公告)号：US20130299720A1

    公开(公告)日：2013-11-14

    申请号：US13986039

    申请日：2013-03-26

    Applicant: Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    Inventor： Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    IPC: C09K11/77 ,  G01T1/20

    CPC classification number: C09K11/7773 ,  C09K11/664 ,  C09K11/7772 ,  G01T1/20 ,  G01T1/202 ,  Y10T428/256 ,  Y10T428/2982

    Abstract: A heterogeneous scintillator material is provided comprising core/shell nanoparticles having a highly hygroscopic or deliquescent halide-based core activated with trivalent Ln3+ or divalent Ln2+ lanthanide ions (Ln=La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) and a stable non-hygroscopic shell thereon. The heterogeneous nanoparticles can comprise highly hygroscopic lanthanide halide (LaBr3, LuI3) cores protected with stable non-hygroscopic LaF3 shells. The heterogeneous nanoparticles can comprise deliquescent alkaline earth halide (SrI2, BaI2) cores protected with stable non-hygroscopic (SrF2, BaF2) shells.

    Abstract translation: 提供了一种异质闪烁体材料，其包括具有由三价Ln3 +或二价Ln2 +镧系元素离子（Ln = La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb）活化的高吸湿性或潮解性卤化物基核心的核/壳纳米颗粒 ，Dy，Ho，Er，Tm，Yb，Lu）和稳定的非吸湿性外壳。 非均相纳米颗粒可以包含用稳定的非吸湿性LaF 3壳保护的高吸湿性镧系元素卤化物（LaBr 3，LuI 3）。 非均相纳米颗粒可以包含用稳定的非吸湿性（SrF 2，BaF 2）壳保护的潮解性碱土卤​​化物（SrI 2，BaI 2）。

    Lead-iodide-based scintillator materials
    2.
    发明申请
    Lead-iodide-based scintillator materials 审中-公开
    基于碘化铅的闪烁体材料

    公开(公告)号：US20100072374A1

    公开(公告)日：2010-03-25

    申请号：US12383953

    申请日：2009-03-30

    Applicant: Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    Inventor： Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    IPC: G01T1/20 ,  C01B11/22

    CPC classification number: G01T1/2023 ,  C01B9/06 ,  C01G21/00 ,  C01P2002/72 ,  C01P2002/82 ,  C01P2004/03 ,  C01P2004/04 ,  C01P2004/62 ,  C01P2006/10

    Abstract: Scintillator material comprising nanoparticles (nanocrystals) comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) wherein the nanoparticles exhibit room-temperature scintillation under gamma irradiation. The scintillator nanoparticles can comprise Pb3O2I2. The scintillator nanoparticles can comprise PbIOH in generally equiatomic proportions or non-equiatomic variants thereof that exhibit scintillation under gamma irradiation. The scintillator nanoparticles have a particle dimension in the range of about 5 to about 100 nm. Microparticles (microcrystals) also are provided comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) grown in a nanoparticle colloidal solution over time to a particle dimension greater than 0.1 μm, such as about 2 microns.

    Abstract translation: 包含包含铅（Pb），碘（I）和任选的氧（O）和氢（H）中的一种或两者的纳米颗粒（纳米晶体）的闪烁体材料，其中纳米颗粒在γ照射下呈现室温闪烁。 闪烁体纳米颗粒可以包含Pb 3 O 2 I 2。 闪烁体纳米颗粒可以包含通常等原子比例的PbIOH或在γ照射下显示闪烁的非等摩尔变体。 闪烁体纳米颗粒具有在约5至约100nm范围内的粒子尺寸。 还提供包含铅（Pb），碘（I）以及任选的在纳米颗粒胶体溶液中生长的氧（O）和氢（H）中的一种或两种随时间推移至微米尺寸大于0.1μm的微粒（微晶） 例如约2微米。

    Halide-based scintillator nanomaterial
    3.
    发明申请
    Halide-based scintillator nanomaterial 有权
    卤化物闪烁体纳米材料

    公开(公告)号：US20100001209A1

    公开(公告)日：2010-01-07

    申请号：US12386503

    申请日：2009-04-17

    Applicant: Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    Inventor： Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    IPC: G01J1/58 ,  C09K11/61

    CPC classification number: C09K11/7773 ,  C09K11/664 ,  C09K11/7772 ,  G01T1/20 ,  G01T1/202 ,  Y10T428/256 ,  Y10T428/2982

    Abstract: Scintillator material comprising nanoparticles (nanocrystals) comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) wherein the nanoparticles exhibit room-temperature scintillation under gamma irradiation. The scintillator nanoparticles can comprise Pb3O2I2. The scintillator nanoparticles can comprise PbIOH in generally equiatomic proportions or non-equiatomic variants thereof that exhibit scintillation under gamma irradiation. The scintillator nanoparticles have a particle dimension in the range of about 5 to about 100 nm. Microparticles (microcrystals) also are provided comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) grown in a nanoparticle colloidal solution over time to a particle dimension greater than 0.1 μm, such as about 2 microns. A heterogeneous scintillator material is provided comprising core/shell nanoparticles having a highly hygroscopic or deliquescent halide-based core activated with trivalent Ln3+ or divalent Ln2+ lanthanide ions (Ln=La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) and a stable non-hygroscopic shell thereon. The heterogeneous nanoparticles can comprise highly hygroscopic lanthanide halide (LaBr3, LuI3) cores protected with stable non-hygroscopic LaF3 shells. The heterogeneous nanoparticles can comprise deliquescent alkaline earth halide (SrI2, BaI2) cores protected with stable non-hygroscopic (SrF2, BaF2) shells.

    Abstract translation: 包含包含铅（Pb），碘（I）和任选的氧（O）和氢（H）中的一种或两者的纳米颗粒（纳米晶体）的闪烁体材料，其中纳米颗粒在γ照射下呈现室温闪烁。 闪烁体纳米颗粒可以包含Pb 3 O 2 I 2。 闪烁体纳米颗粒可以包含通常等原子比例的PbIOH或在γ照射下显示闪烁的非等摩尔变体。 闪烁体纳米颗粒具有在约5至约100nm范围内的粒子尺寸。 还提供包含铅（Pb），碘（I）以及任选的在纳米颗粒胶体溶液中生长的氧（O）和氢（H）中的一种或两种随时间变化至大于0.1μm的颗粒尺寸的微颗粒（微晶） 例如约2微米。 提供了一种异质闪烁体材料，其包括具有由三价Ln3 +或二价Ln2 +镧系元素离子（Ln = La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb）活化的高吸湿性或潮解性卤化物基核心的核/壳纳米颗粒 ，Dy，Ho，Er，Tm，Yb，Lu）和稳定的非吸湿性外壳。 非均相纳米颗粒可以包含用稳定的非吸湿性LaF 3壳保护的高吸湿性镧系元素卤化物（LaBr 3，LuI 3）。 非均相纳米颗粒可以包含用稳定的非吸湿性（SrF 2，BaF 2）壳保护的潮解性碱土卤​​化物（SrI 2，BaI 2）。

    Halide-based scintillator nanomaterial
    5.
    发明授权
    Halide-based scintillator nanomaterial 有权
    卤化物闪烁体纳米材料

    公开(公告)号：US08431041B2

    公开(公告)日：2013-04-30

    申请号：US12386503

    申请日：2009-04-17

    Applicant: Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    Inventor： Marek A. Osinski ,  Nathan J. Withers ,  Brian A. Akins ,  Gennady A. Smolyakov ,  Krishnaprasad Sankar

    IPC: C09K11/08 ,  C09K11/61

    CPC classification number: C09K11/7773 ,  C09K11/664 ,  C09K11/7772 ,  G01T1/20 ,  G01T1/202 ,  Y10T428/256 ,  Y10T428/2982

    Abstract: Scintillator material comprising nanoparticles (nanocrystals) comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) wherein the nanoparticles exhibit room-temperature scintillation under gamma irradiation. The scintillator nanoparticles can comprise Pb3O2I2. The scintillator nanoparticles can comprise PbIOH in generally equiatomic proportions or non-equiatomic variants thereof that exhibit scintillation under gamma irradiation. The scintillator nanoparticles have a particle dimension in the range of about 5 to about 100 nm. Microparticles (microcrystals) also are provided comprising lead (Pb), iodine (I), and optionally one or both of oxygen (O) and hydrogen (H) grown in a nanoparticle colloidal solution over time to a particle dimension greater than 0.1 μm, such as about 2 microns. A heterogeneous scintillator material is provided comprising core/shell nanoparticles having a highly hygroscopic or deliquescent halide-based core activated with trivalent Ln3+ or divalent Ln2+ lanthanide ions (Ln=La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) and a stable non-hygroscopic shell thereon. The heterogeneous nanoparticles can comprise highly hygroscopic lanthanide halide (LaBr3, LuI3) cores protected with stable non-hygroscopic LaF3 shells. The heterogeneous nanoparticles can comprise deliquescent alkaline earth halide (SrI2, BaI2) cores protected with stable non-hygroscopic (SrF2, BaF2) shells.

    Abstract translation: 包含包含铅（Pb），碘（I）和任选的氧（O）和氢（H）中的一种或两者的纳米颗粒（纳米晶体）的闪烁体材料，其中纳米颗粒在γ照射下呈现室温闪烁。 闪烁体纳米颗粒可以包含Pb 3 O 2 I 2。 闪烁体纳米颗粒可以包含通常等原子比例的PbIOH或在γ照射下显示闪烁的非等摩尔变体。 闪烁体纳米颗粒具有在约5至约100nm范围内的粒子尺寸。 还提供包含铅（Pb），碘（I）以及任选的在纳米颗粒胶体溶液中生长的氧（O）和氢（H）中的一种或两种随时间变化至大于0.1μm的颗粒尺寸的微颗粒（微晶） 例如约2微米。 提供了一种异质闪烁体材料，其包括具有由三价Ln3 +或二价Ln2 +镧系元素离子（Ln = La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb）活化的高吸湿性或潮解性卤化物基核心的核/壳纳米颗粒 ，Dy，Ho，Er，Tm，Yb，Lu）和稳定的非吸湿性外壳。 非均相纳米颗粒可以包含用稳定的非吸湿性LaF 3壳保护的高吸湿性镧系元素卤化物（LaBr 3，LuI 3）。 非均相纳米颗粒可以包含用稳定的非吸湿性（SrF 2，BaF 2）壳保护的潮解性碱土卤​​化物（SrI 2，BaI 2）。

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