公开(公告)号：US20150307363A1

公开(公告)日：2015-10-29

申请号：US14649092

申请日：2013-11-27

申请人： Min-Zae OH ,  Jens HAUBROCK ,  Thorsten SCHWAERTZKE ,  Imad MOUSSALLEM ,  Martin TROCHA

发明人： Min-Zae OH ,  Jens HAUBROCK ,  Thorsten SCHWAERTZKE ,  Imad MOUSSALLEM ,  Martin TROCHA

IPC分类号： C01B33/04

CPC分类号： C01B33/04 ,  C01B3/0015 ,  C01B6/006 ,  C01B33/107 ,  Y02E60/328

摘要： The present invention relates to a continuous process for hydrogenating halogen-containing silane compounds having at least three silicon atoms, in which at least one halogen-containing silane compound having at least three silicon atoms and at least one hydrogenating agent are converted continuously to form at least one hydridosilane compound having at least 3 silicon atoms and oxidized hydrogenating agent, and wherein oxidized hydrogenating agent is withdrawn and reduced, and the reaction product of this reduction reaction is sent back to the hydrogenation, to the hydridosilane compounds obtainable by this process and to the use thereof.

摘要翻译： 本发明涉及一种用于氢化含有至少三个硅原子的含卤素的硅烷化合物的连续方法，其中至少一种具有至少三个硅原子的含卤素的硅烷化合物和至少一种氢化剂被连续地转化成 至少一个具有至少3个硅原子的氢硅烷化合物和氧化的氢化剂，并且其中将氧化的氢化剂排出并还原，并将该还原反应的反应产物送回氢化，得到可通过该方法获得的氢硅烷化合物， 其使用。

公开(公告)号：US09561965B2

公开(公告)日：2017-02-07

申请号：US14649092

申请日：2013-11-27

申请人： Min-Zae Oh ,  Jens Haubrock ,  Thorsten Schwaertzke ,  Imad Moussallem ,  Martin Trocha

发明人： Min-Zae Oh ,  Jens Haubrock ,  Thorsten Schwaertzke ,  Imad Moussallem ,  Martin Trocha

IPC分类号： B01J29/90 ,  C01B33/04 ,  C01B3/00 ,  C01B33/107

CPC分类号： C01B33/04 ,  C01B3/0015 ,  C01B6/006 ,  C01B33/107 ,  Y02E60/328

摘要： The present invention relates to a continuous process for hydrogenating halogen-containing silane compounds having at least three silicon atoms, in which at least one halogen-containing silane compound having at least three silicon atoms and at least one hydrogenating agent are converted continuously to form at least one hydridosilane compound having at least 3 silicon atoms and oxidized hydrogenating agent, and wherein oxidized hydrogenating agent is withdrawn and reduced, and the reaction product of this reduction reaction is sent back to the hydrogenation, to the hydridosilane compounds obtainable by this process and to the use thereof.

摘要翻译： 本发明涉及一种用于氢化含有至少三个硅原子的含卤素的硅烷化合物的连续方法，其中至少一种具有至少三个硅原子的含卤素的硅烷化合物和至少一种氢化剂被连续地转化成 至少一个具有至少3个硅原子的氢硅烷化合物和氧化的氢化剂，并且其中将氧化的氢化剂排出并还原，并将该还原反应的反应产物送回氢化，得到可通过该方法获得的氢硅烷化合物， 其使用。

公开(公告)号：US09011812B2

公开(公告)日：2015-04-21

申请号：US13991986

申请日：2011-12-20

申请人： Nicole Brausch ,  Jens Haubrock ,  Udo Knippenberg ,  Thorsten Schwaertzke ,  Joerg Zoellner ,  Stephan Wieber

发明人： Nicole Brausch ,  Jens Haubrock ,  Udo Knippenberg ,  Thorsten Schwaertzke ,  Joerg Zoellner ,  Stephan Wieber

IPC分类号： C01B33/04 ,  C01B33/107

CPC分类号： C01B33/107 ,  C01B33/04 ,  C01B33/10705 ,  C01B33/1071 ,  C01B33/10768 ,  C01B33/10773

摘要： The present invention relates to a process for preparing hydridosilanes from halosilanes, in which a) i) at least one halosilane of the generic formula SinX2n+2 (where n≧3 and X=F, Cl, Br and/or I) and ii) at least one catalyst are converted to form a mixture comprising at least one halosilane of the generic formula SimX2m+2 (where m>n and X=F, Cl, Br and/or I) and SiX4 (where X=F, Cl, Br and/or I), and b) the at least one halosilane of the generic formula SimX2m+2 is hydrogenated to form a hydridosilane of the generic formula SimH2m+2, the hydridosilane of the generic formula SimH2m+2 is separated from partially halogenated hydridosilanes of the general formula SimH(2m+2−y)Xy (where 1

摘要翻译： 本发明涉及一种由卤代硅烷制备氢硅烷的方法，其中a）i）至少一种通式为SinX2n + 2的卤代硅烷（其中n≥3且X = F，Cl，Br和/或I）和ii ）将至少一种催化剂转化成形成包含至少一种通式SimX2m + 2的卤代硅烷（其中m> n和X = F，Cl，Br和/或I）和SiX 4（其中X = F，Cl ，Br和/或I），和b）将通式SimX2m + 2的至少一种卤代硅烷氢化形成通式SimH 2 m + 2的氢硅烷，通式SimH 2 m + 2的氢硅烷与部分 通式SimH（2m + 2-y）Xy（其中1

公开(公告)号：US20130259791A1

公开(公告)日：2013-10-03

申请号：US13991986

申请日：2011-12-20

申请人： Nicole Brausch ,  Jens Haubrock ,  Udo Knippenberg ,  Thorsten Schwaertzke ,  Joerg Zoellner ,  Stephan Wieber

发明人： Nicole Brausch ,  Jens Haubrock ,  Udo Knippenberg ,  Thorsten Schwaertzke ,  Joerg Zoellner ,  Stephan Wieber

IPC分类号： C01B33/107

CPC分类号： C01B33/107 ,  C01B33/04 ,  C01B33/10705 ,  C01B33/1071 ,  C01B33/10768 ,  C01B33/10773

摘要： The present invention relates to a process for preparing hydridosilanes from halosilanes, in which a) i) at least one halosilane of the generic formula SinX2n+2 (where n≧3 and X=F, Cl, Br and/or I) and ii) at least one catalyst are converted to form a mixture comprising at least one halosilane of the generic formula SimX2m+2 (where m>n and X=F, Cl, Br and/or I) and SiX4 (where X=F, Cl, Br and/or I), and b) the at least one halosilane of the generic formula SimX2m+2 is hydrogenated to form a hydridosilane of the generic formula SimH2m+2, the hydridosilane of the generic formula SimH2m+2 is separated from partially halogenated hydridosilanes of the general formula SimH(2m+2−y)Xy (where 1

摘要翻译： 本发明涉及一种由卤代硅烷制备氢硅烷的方法，其中a）i）至少一种通式为SinX2n + 2（其中n≥3且X = F，Cl，Br和/或I）的卤代硅烷和 ii）将至少一种催化剂转化成包含至少一种通式SimX2m + 2的卤代硅烷（其中m> n和X = F，Cl，Br和/或I）和SiX 4（其中X = F， Cl，Br和/或I），和b）将通式SimX2m + 2的至少一种卤代硅烷氢化形成通式SimH2m + 2的氢硅烷，通式SimH2m + 2的氢硅烷与 通式SimH（2m + 2-y）Xy（其中1