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公开(公告)号：US20080105085A1
公开(公告)日：2008-05-08
申请号：US11664640
申请日：2005-10-13
申请人： Insoo Kim , Chang Gun Lee , Sang Ho Kim , Charles E. Smith , Young Jin Kim
发明人： Insoo Kim , Chang Gun Lee , Sang Ho Kim , Charles E. Smith , Young Jin Kim
IPC分类号： B22F9/00
CPC分类号： B22F9/30 , B22F2998/10 , B22F2999/00 , B22F1/0003 , B22F2202/01
摘要： A method for synthesizing high purity silver particles and colloids without requiring the addition of either surfactants or reducing agents thereto, or requiring only a minimal amount thereof. The synthesizing process comprises: (i) a silver oxalate synthesizing process; (ii) a process of dispersing silver oxalate into an appropriate carrier; and {iii) a process of heating said silver oxalate dispersed into said carrier at a temperature of at least 100° C. Silver particles and colloids of various form factor and size may be synthesized depending upon the reaction conditions, the carrier, and the type of surfactant.
摘要翻译： 合成高纯度银粒子和胶体的方法，而不需要向其中加入表面活性剂或还原剂，或仅需要最少量的。 合成方法包括：（i）草酸银合成方法; （ii）将草酸银分散到合适的载体中的方法; 和（iii）在至少100℃的温度下加热分散在所述载体中的草酸银的方法。根据反应条件，载体和类型，可以合成各种形状因子和大小的银颗粒和胶体 的表面活性剂。
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公开(公告)号：US20050217429A1
公开(公告)日：2005-10-06
申请号：US10814151
申请日：2004-04-01
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , B22F2999/00 , Y10S977/896 , B22F2202/01
摘要： The present invention is directed to methods for forming nanosized metal particles. Preferably, nanosized noble metal particles are formed. According to the methods of the invention, a product containing nanosized metal particles in a solvent are formed. Additionally, processing to remove undesirable byproducts created or used during the fabrication process are not necessary.
摘要翻译： 本发明涉及形成纳米尺寸金属颗粒的方法。 优选地，形成纳米尺寸的贵金属颗粒。 根据本发明的方法，形成在溶剂中含有纳米尺寸金属颗粒的产品。 此外，不需要在制造过程中产生或使用的去除不期望的副产物的处理。
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3.发明授权公开(公告)号：US08557217B2
公开(公告)日：2013-10-15
申请号：US12310615
申请日：2007-09-11
申请人： Insoo Kim , Woo Jin Lee , Young Jin Kim , Charles E. Smith, Jr.
发明人： Insoo Kim , Woo Jin Lee , Young Jin Kim , Charles E. Smith, Jr.
IPC分类号： C01G23/053 , C01B15/01
CPC分类号： C01G23/053 , B82Y30/00 , C01G23/0532 , C01G23/0536 , C01P2002/72 , C01P2004/03 , C01P2004/50 , C01P2004/64
摘要： A process for synthesizing nano-sized rutile, anatase, or a mixture of rutile and anatase TiO2 powder. The process includes the steps of: 1) forming a Ti-peroxo complex by mixing H2O2 with a Ti compound, and 2) heating the Ti-peroxo complex at a temperature of above 50° C. A primary particle size of TiO2 particles, synthesized by the method, is below 50 nm, and an agglomerated particle size thereof after a washing/dry process is below about 10 μm. The major characteristics of the present invention are that it is a low temperature process, a highly concentrated synthesis, and high production yield of above 90%.
摘要翻译： 合成纳米尺寸金红石，锐钛矿或金红石和锐钛矿TiO 2粉末的混合物的方法。 该方法包括以下步骤：1）通过将H 2 O 2与Ti化合物混合形成Ti-过氧配合物，和2）在高于50℃的温度下加热Ti-过氧配合物。合成的TiO 2颗粒的一次粒径 通过该方法，低于50nm，洗涤/干燥处理后的附聚粒径低于约10μm。 本发明的主要特征是低温工艺，高浓缩合成，高产率高于90％。
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公开(公告)号：US20080064592A1
公开(公告)日：2008-03-13
申请号：US11664711
申请日：2005-10-13
申请人： Insoo Kim , Gang Kim , Young Choi , Woo Lee , Charles Smith Jr. , Young Kim
发明人： Insoo Kim , Gang Kim , Young Choi , Woo Lee , Charles Smith Jr. , Young Kim
IPC分类号： C02F1/42 , C01G23/047
CPC分类号： C01G23/053 , C01G23/04 , C01G23/0532 , C01G23/0536 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C01P2004/64 , C09C1/3661
摘要： A method for synthesizing TiO2, metal-doped TiO2, and metal-coated TiO2 particles of spherical form factor and needle type of which the average particle size is below 150 nm. The method of the invention is to synthesize Ti(OH)4, metal-doped Ti(OH)4 or metal-coated Ti(OH)4, and react the same by applying a pressure above the saturated vapor pressure at a temperature above 100° C. The pressure is achieved by means of the pressure of the vapor generated during the reaction inside of a closed reactor, by pressure applied from the outside, or a mixture of both. Gases to increase the pressure from outside are preferably inert gases such as Ar and N2 but are not limited to inert gases.
摘要翻译： 用于合成TiO 2，金属掺杂TiO 2和金属涂覆的球形形状和针型的TiO 2颗粒的方法，其中 平均粒径低于150nm。 本发明的方法是合成Ti（OH）4 N，金属掺杂的Ti（OH）4或金属涂覆的Ti（OH）4，并通过施加高于饱和的 在高于100℃的温度下的蒸汽压力。压力通过在封闭反应器内部的反应期间产生的蒸气的压力，通过从外部施加的压力或两者的混合物来实现。 从外部增加压力的气体优选为惰性气体，例如Ar和N 2，但不限于惰性气体。
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公开(公告)号：US09545668B2
公开(公告)日：2017-01-17
申请号：US13511424
申请日：2010-10-12
申请人： Insoo Kim , Chang-Gun Lee , Tomoki Kitafuji
发明人： Insoo Kim , Chang-Gun Lee , Tomoki Kitafuji
CPC分类号： B22F1/0062 , B22F1/0018 , B22F1/0059 , B22F1/0081 , B22F1/02 , B22F9/26 , B22F2001/0033 , B82Y30/00 , H01B1/02 , H01B1/22 , Y10T428/2991
摘要： A fine silver particle-containing composition includes a large number of fine silver particles 2 and a coating layer 4 that covers a surface of each silver particle 2. The silver particle 2 is a so-called nano particle. The silver particle 2 has a scale-like shape. The coating layer 4 consists of an organic compound. The organic compound binds to the silver particle 2. The organic compound suppresses aggregation of the silver particle 2. The composition is in a cake form. A weight ratio of the organic compound with regard to the total amount of the composition is not lower than 2% but not higher than 15%.
摘要翻译： 含有银颗粒的组合物包括大量细银颗粒2和覆盖每个银颗粒2的表面的涂层4.银颗粒2是所谓的纳米颗粒。 银颗粒2具有鳞片形状。 涂层4由有机化合物组成。 有机化合物与银颗粒2结合。有机化合物抑制银颗粒2的聚集。组合物为饼形。 有机化合物相对于组合物总量的重量比不低于2％但不高于15％。
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6.发明申请公开(公告)号：US20100226851A1
公开(公告)日：2010-09-09
申请号：US12310615
申请日：2007-09-11
申请人： Insoo Kim , Woo Jin Lee , Young Jin Kim , Charles E. Smith, JR.
发明人： Insoo Kim , Woo Jin Lee , Young Jin Kim , Charles E. Smith, JR.
IPC分类号： C01G23/047
CPC分类号： C01G23/053 , B82Y30/00 , C01G23/0532 , C01G23/0536 , C01P2002/72 , C01P2004/03 , C01P2004/50 , C01P2004/64
摘要： A process for synthesizing nano-sized rutile, anatase, or a mixture of rutile and anatase TiO2 powder. The process includes the steps of: 1) forming a Ti-peroxo complex by mixing H2O2 with a Ti compound, and 2) heating the Ti-peroxo complex at a temperature of above 50° C. A primary particle size of TiO2 particles, synthesized by the method, is below 50 nm, and an agglomerated particle size thereof after a washing/dry process is below about 10 μm. The major characteristics of the present invention are that it is a low temperature process, a highly concentrated synthesis, and high production yield of above 90%.
摘要翻译： 合成纳米尺寸金红石，锐钛矿或金红石和锐钛矿TiO 2粉末的混合物的方法。 该方法包括以下步骤：1）通过将H 2 O 2与Ti化合物混合形成Ti-过氧配合物，和2）在高于50℃的温度下加热Ti-过氧配合物。合成的TiO 2颗粒的一次粒径 通过该方法低于50nm，洗涤/干燥处理后的附聚粒径低于约10μm。 本发明的主要特征是低温工艺，高浓缩合成，高产率高于90％。
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公开(公告)号：US20120280187A1
公开(公告)日：2012-11-08
申请号：US13511424
申请日：2010-10-12
申请人： Insoo Kim , Chang-Gun Lee , Tomoki Kitafuji
发明人： Insoo Kim , Chang-Gun Lee , Tomoki Kitafuji
CPC分类号： B22F1/0062 , B22F1/0018 , B22F1/0059 , B22F1/0081 , B22F1/02 , B22F9/26 , B22F2001/0033 , B82Y30/00 , H01B1/02 , H01B1/22 , Y10T428/2991
摘要： A fine silver particle-containing composition includes a large number of fine silver particles 2 and a coating layer 4 that covers a surface of each silver particle 2. The silver particle 2 is a so-called nano particle. The silver particle 2 has a scale-like shape. The coating layer 4 consists of an organic compound. The organic compound binds to the silver particle 2. The organic compound suppresses aggregation of the silver particle 2. The composition is in a cake form. A weight ratio of the organic compound with regard to the total amount of the composition is not lower than 2% but not higher than 15%.
摘要翻译： 含有银颗粒的组合物包括大量细银颗粒2和覆盖每个银颗粒2的表面的涂层4.银颗粒2是所谓的纳米颗粒。 银颗粒2具有鳞片形状。 涂层4由有机化合物组成。 有机化合物与银颗粒2结合。有机化合物抑制银颗粒2的聚集。组合物为饼形。 有机化合物相对于组合物总量的重量比不低于2％但不高于15％。
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公开(公告)号：US07270695B2
公开(公告)日：2007-09-18
申请号：US10814151
申请日：2004-04-01
申请人： Insoo Kim , Gang Hyuk Kim , Chang Gun Lee , Young Jin Kim , Charles Smith
发明人： Insoo Kim , Gang Hyuk Kim , Chang Gun Lee , Young Jin Kim , Charles Smith
IPC分类号： B22F9/24
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , B22F2999/00 , Y10S977/896 , B22F2202/01
摘要： The present invention is directed to methods for forming nanosized metal particles. Preferably, nanosized noble metal particles are formed. According to the methods of the invention, a product containing nanosized metal particles in a solvent are formed. Additionally, processing to remove undesirable byproducts created or used during the fabrication process are not necessary.
摘要翻译： 本发明涉及形成纳米尺寸金属颗粒的方法。 优选地，形成纳米尺寸的贵金属颗粒。 根据本发明的方法，形成在溶剂中含有纳米尺寸金属颗粒的产品。 此外，不需要在制造过程中产生或使用的去除不期望的副产物的处理。
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