公开(公告)号：US5850623A

公开(公告)日：1998-12-15

申请号：US947689

申请日：1997-10-09

申请人： Howard Smith Carman, Jr. ,  Daniel Charles Alsmeyer ,  Carlos Humberto Juarez-Garcia ,  Aaron Wayne Garrett ,  Bruce Edwin Wilson ,  Vincent Alvin Nicely

发明人： Howard Smith Carman, Jr. ,  Daniel Charles Alsmeyer ,  Carlos Humberto Juarez-Garcia ,  Aaron Wayne Garrett ,  Bruce Edwin Wilson ,  Vincent Alvin Nicely

IPC分类号： G01J3/28 ,  G01J3/44 ,  G01N21/27 ,  G01N21/65 ,  G01N33/00

CPC分类号： G01J3/44 ,  G01J3/28 ,  G01N21/65 ,  G01J2003/2866 ,  G01N21/278

摘要： A method for providing a standard Raman spectrum from a sample uses a particular Raman spectrometry apparatus or any similar Raman spectrometry apparatus, which is used to simultaneously irradiate a reference material and at least one sample, thereby obtaining their respective convolved Raman spectra. Using a defined standard energy dispersion characteristic and a standard Raman spectrum of the reference material, a convolution function is determined and applied to produce a deconvolved Raman spectrum of the sample. This deconvolved spectrum is multiplied by a defined standard photometric response function to produce a standard Raman spectrum of the sample. A method for providing an accurate and precise quantitative analysis of the chemical composition and/or physical properties of an unknown sample uses the standard Raman spectra of a plurality of known samples to construct a normalized calibration, which is applied to a standard Raman spectrum of the unknown sample to produce an accurate and precise quantitative analysis thereof, using any similar Raman spectrometry apparatus.

摘要翻译： 用于从样品提供标准拉曼光谱的方法使用特定的拉曼光谱测定装置或任何类似的拉曼光谱测定装置，其用于同时照射参考材料和至少一个样品，从而获得它们各自的卷积拉曼光谱。 使用定义的标准能量色散特征和参考物质的标准拉曼光谱，确定并应用卷积函数以产生样品的解卷积拉曼光谱。 该解卷积乘以所定义的标准光度响应函数，以产生样品的标准拉曼光谱。 提供对未知样品的化学组成和/或物理性质的准确和精确的定量分析的方法使用多个已知样品的标准拉曼光谱来构建归一化校准，其应用于标准拉曼光谱 未知样品，以使用任何类似的拉曼光谱测定装置产生精确和精确的定量分析。

公开(公告)号：US20100273956A1

公开(公告)日：2010-10-28

申请号：US12430470

申请日：2009-04-27

申请人： Jason Christopher Jenkins ,  Gary Wayne Connell ,  Howard Smith Carman, JR. ,  Douglas Weldon Carico, JR. ,  Jimmy Ray Trotter ,  Alan Wayne White ,  Mary Therese Jernigan ,  Rodney Scott Armentrout

发明人： Jason Christopher Jenkins ,  Gary Wayne Connell ,  Howard Smith Carman, JR. ,  Douglas Weldon Carico, JR. ,  Jimmy Ray Trotter ,  Alan Wayne White ,  Mary Therese Jernigan ,  Rodney Scott Armentrout

IPC分类号： C08G63/692 ,  C08G63/84

CPC分类号： C08G63/84 ,  C08G63/183 ,  C08K5/49 ,  Y10T428/294 ,  Y10T428/31681 ,  Y10T428/31978 ,  C08L67/02

摘要： Processes for producing polyethylene terephthalate copolyesters are disclosed, that include the steps of: esterifying a mixture of at least terephthalic acid, from 20 mole percent to 45 mole percent 1,4-cyclohexanedimethanol, and ethylene glycol, optionally in the presence of one or more alkaline earth metals or alkali metals, to form an oligomer; polycondensing the oligomer in the melt phase in the presence of aluminum and one or more alkaline earth metals or alkali metals, to obtain a copolyester having an intrinsic viscosity of at least 0.5 dL/g; and thereafter adding to the copolyester a phosphorus-containing compound.

摘要翻译： 公开了用于生产聚对苯二甲酸乙二醇酯共聚酯的方法，其包括以下步骤：任选地在一种或多种存在下将至少对苯二甲酸，20摩尔％至45摩尔％的1,4-环己烷二甲醇和乙二醇的混合物酯化 碱土金属或碱金属，形成低聚物; 在铝和一种或多种碱土金属或碱金属的存在下，在熔融相中使低聚物缩聚，得到特性粘度至少为0.5dL / g的共聚酯; 然后向共聚酯中加入含磷化合物。

公开(公告)号：US07915374B2

公开(公告)日：2011-03-29

申请号：US12430470

申请日：2009-04-27

申请人： Jason Christopher Jenkins ,  Gary Wayne Connell ,  Howard Smith Carman, Jr. ,  Douglas Weldon Carico, Jr. ,  Jimmy Ray Trotter ,  Alan Wayne White ,  Mary Therese Jernigan ,  Rodney Scott Armentrout

发明人： Jason Christopher Jenkins ,  Gary Wayne Connell ,  Howard Smith Carman, Jr. ,  Douglas Weldon Carico, Jr. ,  Jimmy Ray Trotter ,  Alan Wayne White ,  Mary Therese Jernigan ,  Rodney Scott Armentrout

IPC分类号： C08G63/00 ,  C08G63/02

CPC分类号： C08G63/84 ,  C08G63/183 ,  C08K5/49 ,  Y10T428/294 ,  Y10T428/31681 ,  Y10T428/31978 ,  C08L67/02

摘要： Processes for producing polyethylene terephthalate copolyesters are disclosed, that include the steps of: esterifying a mixture of at least terephthalic acid, from 20 mole percent to 45 mole percent 1,4-cyclohexanedimethanol, and ethylene glycol, optionally in the presence of one or more alkaline earth metals or alkali metals, to form an oligomer; polycondensing the oligomer in the melt phase in the presence of aluminum and one or more alkaline earth metals or alkali metals, to obtain a copolyester having an intrinsic viscosity of at least 0.5 dL/g; and thereafter adding to the copolyester a phosphorus-containing compound.

摘要翻译： 公开了用于生产聚对苯二甲酸乙二醇酯共聚酯的方法，其包括以下步骤：任选地在一种或多种存在下将至少对苯二甲酸，20摩尔％至45摩尔％的1,4-环己烷二甲醇和乙二醇的混合物酯化 碱土金属或碱金属，形成低聚物; 在铝和一种或多种碱土金属或碱金属的存在下，在熔融相中使低聚物缩聚，得到特性粘度至少为0.5dL / g的共聚酯; 然后向共聚酯中加入含磷化合物。