公开(公告)号：US10100386B2

公开(公告)日：2018-10-16

申请号：US13523941

申请日：2012-06-15

Applicant: Andrew Philip Woodfield ,  Eric Allen Ott ,  Clifford Earl Shamblen ,  Michael Francis Xavier Gigliotti

Inventor： Andrew Philip Woodfield ,  Eric Allen Ott ,  Clifford Earl Shamblen ,  Michael Francis Xavier Gigliotti

IPC: B22F1/02 ,  C22B34/12 ,  B22F3/00 ,  B22F9/18 ,  B22F9/20 ,  B22F9/28 ,  C21B13/00 ,  C21B13/14 ,  C22B5/12 ,  C22C1/04 ,  C22C1/10 ,  C22B4/06

Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.

公开(公告)号：US20120263619A1

公开(公告)日：2012-10-18

申请号：US13523941

申请日：2012-06-15

Applicant: Andrew Philip WOODFIELD ,  Eric Allen OTT ,  Clifford Earl SHAMBLEN ,  Michael Francis Xavier GIGLIOTTI

Inventor： Andrew Philip WOODFIELD ,  Eric Allen OTT ,  Clifford Earl SHAMBLEN ,  Michael Francis Xavier GIGLIOTTI

IPC: B22F1/00 ,  C22C1/00

CPC classification number: C22B34/1263 ,  B22F1/02 ,  B22F3/001 ,  B22F9/18 ,  B22F9/20 ,  B22F9/28 ,  B22F2998/00 ,  B22F2999/00 ,  C21B13/006 ,  C21B13/146 ,  C22B4/06 ,  C22B5/12 ,  C22B34/129 ,  C22B34/1295 ,  C22C1/04 ,  C22C1/0433 ,  C22C1/0458 ,  C22C1/10 ,  C22C2001/1089 ,  B22F3/12 ,  B22F3/15 ,  B22F3/17 ,  B22F3/20

Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.

Abstract translation: 制备与合金元素合金的母材的制品的方法包括以下步骤：通过提供化学还原的贱金属的非金属贱金属前体化合物制备复合混合物，提供化学还原的非金属合金元素 合金元素的前体化合物，然后混合贱金属前体化合物和合金元素前体化合物以形成化合物混合物。 然后将复合混合物还原成金属合金，而不熔化金属合金。 制备步骤或化学还原步骤包括添加其它添加剂成分的步骤。 然后将金属合金固结，生产固结的金属制品，而不会熔化金属合金，而不熔化固结的金属制品。

公开(公告)号：US07967924B2

公开(公告)日：2011-06-28

申请号：US11130764

申请日：2005-05-17

Applicant: Jon Raymond Groh ,  Eric Allen Ott ,  Robert Edward Schafrik ,  Daniel Donald Krueger

Inventor： Jon Raymond Groh ,  Eric Allen Ott ,  Robert Edward Schafrik ,  Daniel Donald Krueger

IPC: B23P15/04

CPC classification number: F01D5/02 ,  B22F3/004 ,  B22F3/1208 ,  B22F5/009 ,  B22F7/06 ,  B22F2998/00 ,  B22F2998/10 ,  B22F2999/00 ,  B23P15/006 ,  F01D25/005 ,  F05C2253/24 ,  F05D2230/22 ,  F05D2230/311 ,  F05D2230/312 ,  Y02T50/671 ,  Y10T29/4932 ,  Y10T29/49325 ,  B22F3/15 ,  B22F3/20 ,  B22F3/17 ,  B22F5/08 ,  B22F2207/01 ,  B22F1/0003 ,  B22F3/02 ,  B22F1/0085 ,  B22F3/1017 ,  B22F2207/15

Abstract: A compositionally graded gas turbine disk is made by preparing a rotationally symmetric radially inner segment of a gas turbine disk preform, rotating the inner segment about a central axis, spray applying a radially outer-segment material onto the radially inner segment as it rotates about the central axis, preferably achieving a gradual transition in composition, and thereafter further processing the gas turbine disk preform to produce the compositionally graded gas turbine disk.

Abstract translation: 通过制备燃气涡轮盘预制件的旋转对称的径向内部段，通过使内部区段围绕中心轴线旋转来制造成分分级的燃气轮机盘，当径向内部段旋转时，将径向外部段材料喷射到径向内部段上 中心轴，优选地实现组成的逐渐过渡，然后进一步处理燃气涡轮盘预制件以产生组成分级的燃气轮机盘。

公开(公告)号：US07897103B2

公开(公告)日：2011-03-01

申请号：US11140636

申请日：2005-05-27

Applicant: Eric Allen Ott ,  Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Peter Wayte ,  Mike Eugene Mechley

Inventor： Eric Allen Ott ,  Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Peter Wayte ,  Mike Eugene Mechley

IPC: B22F3/02

CPC classification number: B22F5/12 ,  B22F3/001 ,  B22F3/20 ,  B22F8/00 ,  B22F9/18 ,  B22F2998/00 ,  B22F2998/10 ,  B23K35/30 ,  B23K35/325 ,  B23K35/40 ,  C22B9/20 ,  C22B34/1263 ,  C22B34/1295 ,  Y02P10/24 ,  Y02W30/541 ,  B22F9/24 ,  B22F1/0003 ,  B22F3/02 ,  B22F9/20 ,  B22F2207/01 ,  B22F3/1208

Abstract: An elongated rod assembly is made by preparing a plurality of rods. Each rod is prepared by the steps of furnishing at least one nonmetallic precursor compound, thereafter chemically reducing the precursor compounds to produce the metallic material, and thereafter consolidating the metallic material to form the rod, wherein the rod has a rod length equal to the assembly length. The rods are bundled together to form a bundled rod assembly. The rod assembly may be used as a consumable feedstock in a melting-and-casting operation.

Abstract translation: 通过制备多个杆来制造细长杆组件。 每个棒通过以下步骤制备：提供至少一种非金属前体化合物，然后化学还原前体化合物以制备金属材料，然后固结金属材料以形成棒，其中棒具有等于组件的棒长度 长度。 杆被捆绑在一起以形成捆扎杆组件。 棒组件可以用作熔融 - 铸造操作中的可消耗原料。

公开(公告)号：US07833472B2

公开(公告)日：2010-11-16

申请号：US11142786

申请日：2005-06-01

Applicant: Eric Allen Ott ,  Andrew Philip Woodfield ,  David Paul Mourer ,  John Frederick Ackerman ,  Jon Raymond Groh ,  Robert Edward Schafrik ,  Kenneth Rees Bain ,  Michael Francis Xavier Gigliotti ,  Matthew Bernard Buczek

Inventor： Eric Allen Ott ,  Andrew Philip Woodfield ,  David Paul Mourer ,  John Frederick Ackerman ,  Jon Raymond Groh ,  Robert Edward Schafrik ,  Kenneth Rees Bain ,  Michael Francis Xavier Gigliotti ,  Matthew Bernard Buczek

IPC: B22F1/00 ,  B22F1/02

CPC classification number: B22F1/025 ,  B22F2999/00 ,  C23C16/4417 ,  C23C16/442 ,  B22F9/18 ,  B22F9/28

Abstract: An article is prepared by furnishing a plurality of powder particle substrates made of a substrate metal, providing a nonmetallic precursor of a metallic coating material, wherein the metallic coating material comprises an alloying element that is thermophysically melt incompatible with the substrate metal, contacting the powder particle substrates with the nonmetallic precursor, chemically reducing the nonmetallic precursor to form coated powder particles comprising the powder particle substrates having a surface-enriched layer of the metallic coating material thereon without melting the powder particle substrates, and processing the coated powder particles to form the article, without melting the powder particle substrates.

Abstract translation: 通过提供由基底金属制成的多个粉末颗粒基底来制备制品，提供金属涂层材料的非金属前体，其中所述金属涂层材料包括与所述基底金属不相容的热物理熔融的合金元素，使所述粉末接触所述粉末 具有非金属前体的化学还原剂，化学还原非金属前体以形成包含粉末颗粒基质的包覆粉末颗粒，所述粉末颗粒基材具有金属涂层材料的表面富集层，而不熔化粉末颗粒基质，并且处理涂覆的粉末颗粒以形成 制品，不熔化粉末颗粒基质。

公开(公告)号：US07419528B2

公开(公告)日：2008-09-02

申请号：US10371743

申请日：2003-02-19

Applicant: Clifford Earl Shamblen ,  Andrew Philip Woodfield ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

Inventor： Clifford Earl Shamblen ,  Andrew Philip Woodfield ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

IPC: B22F3/00

CPC classification number: B22F3/001 ,  C22C1/0433

Abstract: A metallic article made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds contains more of a base-metal element, such as nickel, cobalt, iron, iron-nickel, and iron-nickel-cobalt than any other metallic element. The mixture of nonmetallic precursor compounds is chemically reduced to produce a metallic superalloy material, without melting the metallic superalloy material. The metallic superalloy material is consolidated to produce a consolidated metallic article, without melting the metallic superalloy material and without melting the consolidated metallic article.

Abstract translation: 由金属构成元件制成的金属制品由金属构成元素的非金属前体化合物的混合物制成。 非金属前体化合物的混合物比任何其它金属元素含有更多的贱金属元素，例如镍，钴，铁，铁 - 镍和铁 - 镍 - 钴。 化学还原非金属前体化合物的混合物以产生金属超耐热合金材料，而不熔化金属超耐热合金材料。 金属超合金材料被固结以产生固结的金属制品，而不熔化金属超合金材料，而不熔化固结的金属制品。

公开(公告)号：US07329381B2

公开(公告)日：2008-02-12

申请号：US10172218

申请日：2002-06-14

Applicant: Andrew Philip Woodfield ,  Eric Allen Ott ,  Clifford Earl Shamblen

Inventor： Andrew Philip Woodfield ,  Eric Allen Ott ,  Clifford Earl Shamblen

IPC: B22F3/12 ,  C22C14/00 ,  C22C19/03 ,  C22C21/00 ,  C22C23/00 ,  C22C32/02 ,  C22C1/04

CPC classification number: C22B34/1295 ,  B22F3/001 ,  B22F9/18 ,  B22F2998/00 ,  C22B4/06 ,  C22B34/1263 ,  B22F9/28 ,  B22F3/12 ,  B22F3/15 ,  B22F3/17 ,  B22F3/20

Abstract: A metallic article made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds is chemically reduced to produce an initial metallic material, without melting the initial metallic material. The initial metallic material is consolidated to produce a consolidated metallic article, without melting the initial metallic material and without melting the consolidated metallic article.

Abstract translation: 由金属构成元件制成的金属制品由金属构成元素的非金属前体化合物的混合物制成。 化学还原非金属前体化合物的混合物以产生初始金属材料，而不熔化初始金属材料。 初始金属材料被固结以产生固结的金属制品，而不熔化初始金属材料并且不熔化固结的金属制品。

公开(公告)号：US07037463B2

公开(公告)日：2006-05-02

申请号：US10329143

申请日：2002-12-23

Applicant: Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

Inventor： Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

IPC: C22C14/00 ,  C22C1/05

CPC classification number: B22F9/24 ,  B22F3/001 ,  B22F9/18 ,  B22F9/20 ,  B22F9/28 ,  C22C1/10 ,  C22C32/0031 ,  C22C2001/1089

Abstract: A metallic article is prepared by first furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively containing the constituent elements of the metallic article in their respective constituent-element proportions. The constituent elements together form a titanium-base alloy having a stable-oxide-forming additive element therein, such as magnesium, calcium, scandium, yttrium, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium, and mixtures thereof. The stable-oxide-forming additive element forms a stable oxide in a titanium-based alloy. At least one additive element is present at a level greater than its room-temperature solid solubility limit in the titanium-base alloy. The precursor compounds are chemically reduced to produce an alloy material, without melting the alloy material. The alloy material may be consolidated. The alloy material, or consolidated metallic article, is thereafter desirably exposed to an oxygen-containing environment at a temperature greater than room temperature.

Abstract translation: 通过首先提供至少一种非金属前体化合物制备金属制品，其中所有非金属前体化合物以其各自的构成元素比例共同含有金属制品的组成元素。 组成元素一起形成其中具有稳定氧化物形成添加元素的钛基合金，例如镁，钙，钪，钇，镧，铈，镨，钕，ium，钐，铕，钆，铽，镝 ，钬，铒，ium，镱和镥，及其混合物。 稳定氧化物形成添加元素在钛基合金中形成稳定的氧化物。 在钛基合金中，至少一种添加元素的含量大于其室温固溶度极限。 前体化合物被化学还原以产生合金材料，而不熔化合金材料。 合金材料可以被固结。 之后，合金材料或固结的金属制品在大于室温的温度下暴露于含氧环境中。

公开(公告)号：US06926755B2

公开(公告)日：2005-08-09

申请号：US10459747

申请日：2003-06-12

Applicant: Clifford Earl Shamblen ,  Andrew Philip Woodfield ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

Inventor： Clifford Earl Shamblen ,  Andrew Philip Woodfield ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

IPC: B22F9/20 ,  B22F9/28 ,  C22C1/04 ,  B22F3/00

CPC classification number: C22C1/0416 ,  B22F9/20 ,  B22F9/28 ,  B22F2998/10 ,  C22C1/04 ,  B22F1/0003

Abstract: An article of aluminum base-metal alloyed with an alloying element is prepared by mixing a chemically reducible nonmetallic base-metal precursor compound of the aluminum base-metal and a chemically reducible nonmetallic alloying-element precursor compound of an alloying element to form a precursor compound mixture. The alloying element may be, but is not necessarily, thermophysically melt incompatible with the aluminum base metal. The method further includes chemically reducing the precursor compound mixture to a metallic alloy, without melting the metallic alloy, and thereafter consolidating the metallic alloy to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.

Abstract translation: 通过将铝基金属的化学还原性非金属贱金属前体化合物和合成元素的化学还原性非金属合金元素前体化合物混合以形成前体化合物来制备与合金元素合金化的铝基金属制品 混合物。 合金元素可以是但不一定是热物理熔融与铝母材不相容的。 该方法还包括将前体化合物混合物化学还原成金属合金，而不熔化金属合金，然后固结金属合金以产生固结的金属制品，而不熔化金属合金并且不熔化固结的金属制品。

公开(公告)号：US08088231B2

公开(公告)日：2012-01-03

申请号：US12834046

申请日：2010-07-12

Applicant: Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

Inventor： Andrew Philip Woodfield ,  Clifford Earl Shamblen ,  Eric Allen Ott ,  Michael Francis Xavier Gigliotti

IPC: C22C14/00

CPC classification number: B22F9/24 ,  B22F3/001 ,  B22F9/18 ,  B22F9/20 ,  B22F9/28 ,  C22C1/10 ,  C22C32/0031 ,  C22C2001/1089

Abstract: A metallic article is prepared by first furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively containing the constituent elements of the metallic article in their respective constituent-element proportions. The constituent elements together form a titanium-base alloy having a stable-oxide-forming additive element therein, such as magnesium, calcium, scandium, yttrium, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium, and mixtures thereof. The stable-oxide-forming additive element forms a stable oxide in a titanium-based alloy. At least one additive element is present at a level greater than its room-temperature solid solubility limit in the titanium-base alloy. The precursor compounds are chemically reduced to produce an alloy material, without melting the alloy material. The alloy material may be consolidated. The alloy material, or consolidated metallic article, is thereafter desirably exposed to an oxygen-containing environment at a temperature greater than room temperature.

Abstract translation: 通过首先提供至少一种非金属前体化合物制备金属制品，其中所有非金属前体化合物以其各自的构成元素比例共同含有金属制品的组成元素。 组成元素一起形成其中具有稳定氧化物形成添加元素的钛基合金，例如镁，钙，钪，钇，镧，铈，镨，钕，ium，钐，铕，钆，铽，镝 ，钬，铒，ium，镱和镥，及其混合物。 稳定氧化物形成添加元素在钛基合金中形成稳定的氧化物。 在钛基合金中，至少一种添加元素的含量大于其室温固溶度极限。 前体化合物被化学还原以产生合金材料，而不熔化合金材料。 合金材料可以被固结。 之后，合金材料或固结的金属制品在大于室温的温度下暴露于含氧环境中。