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1.发明授权公开(公告)号：US06475449B2
公开(公告)日：2002-11-05
申请号：US09754515
申请日：2001-01-04
申请人： Matthias Grehl , Horst Meyer , Dieter Schäfer
发明人： Matthias Grehl , Horst Meyer , Dieter Schäfer
IPC分类号： C22B1100
CPC分类号： C22B3/065 , C01G55/00 , C01G55/004 , C22B3/44 , C22B11/04 , C22B61/00 , Y02P10/234
摘要： A method for extracting osmium and ruthenium from noble metal concentrates, by: a) treatment of a noble metal concentrate containing osmium and ruthenium with nitric acid at a maximum temperature of about T=+30° C., b) heating of the resultant suspension/solution to a minimum temperature of about T=+85° C.; c) capturing the resultant osmium tetroxide in an absorption solution; d) treatment of the suspension/solution having a temperature of about T=+20° C. to 30° C. with hydroxide at a maximum reaction temperature of about T=+65° C.; and e) treatment of the alkaline suspension/solution from step d) with a substance for the oxidizing leaching of the ruthenium.
摘要翻译： 一种从贵金属浓缩物中提取锇和钌的方法，通过以下步骤：a）在约T = + 30℃的最高温度下用硝酸处理含有锇和钌的贵金属浓缩物，b）加热所得悬浮液 /溶液至约T = + 85℃的最低温度; c）在所述吸收溶液中捕获所得的四氧化锇; d）处理温度为约T = + 20℃至30℃的悬浮液/溶液 在约T = + 65℃的最大反应温度下用氢氧化物。 使用步骤d）的碱性悬浮液/溶液处理用于钌氧化浸出的物质。
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公开(公告)号：US06475448B2
公开(公告)日：2002-11-05
申请号：US09753291
申请日：2001-01-02
申请人： Matthias Grehl , Horst Meyer , Dieter Schäfer
发明人： Matthias Grehl , Horst Meyer , Dieter Schäfer
IPC分类号： C22B1100
CPC分类号： C01G55/004 , C22B3/44 , C22B11/00 , Y02P10/234
摘要： Ruthenium is separated from noble metal solutions, by: a) heating a noble metal solution containing ruthenium to a temperature of T=+50° C. to T=+65° C., the H+ concentration and Cl− concentration are greater than 1 mol/l each; b) addition of chlorate, the resulting suspension/solution having a temperature of T=+50° C. to T=+65° C., heating the suspension solution to T=+80° C. to T=+90° C. and passing a carrier gas through the suspension/solution and capturing the resultant ruthenium tetroxide; c) addition of bromate at a pH of 1 to 3, the resultant suspension/solution having a temperature T=+60° C. to T=+95° C., and passing a carrier gas through the suspension solution and capturing the resultant ruthenium tetroxide.
摘要翻译： 钌通过以下方式与贵金属溶液分离：a）将含有钌的贵金属溶液加热至T = + 50℃的温度至T = + 65℃，H +浓度和Cl-浓度大于1 mol / l; b）加入氯酸盐，所得到的悬浮液/溶液的温度为T = + 50℃至T = + 65℃，将悬浮液加热至T = + 80℃至T = + 90℃，并使载气通过悬浮液/溶液并捕获所得的四氧化钌; c）在1至3的pH下加入溴酸盐，所得悬浮液/溶液的温度为T = + 60℃ 至T = + 95℃，并使载气通过悬浮液并捕获所得的四氧化钌。
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公开(公告)号：US08188329B2
公开(公告)日：2012-05-29
申请号：US12056524
申请日：2008-03-27
申请人： Christian Nowottny , Horst Meyer , Matthias Grehl , Dieter Schäfer , Hans-Joachim Alt , Wilhelm Glab
发明人： Christian Nowottny , Horst Meyer , Matthias Grehl , Dieter Schäfer , Hans-Joachim Alt , Wilhelm Glab
CPC分类号： C22B7/001 , C22B11/021 , F23G5/0273 , F23G5/16 , F23G5/50 , F23G7/006 , F23G2207/102 , F23G2207/30 , F23G2208/10 , F23G2209/141 , Y02P10/214
摘要： A recycling furnace and method are provided for processing potentially explosive precious metal-containing materials having organic fractions that combust with great energy, the furnace including a switching facility for alternating operation of a burning-off chamber of the furnace between: (A) pyrolysis or carbonization under protective furnace gas in an atmosphere comprising maximally 6 wt-% oxygen, and (B) oxidative combustion of the organic fractions including carbon. The furnace has indirect heating and a control that determines the end of the pyrolysis or carbonization by a sensor and controls the switching facility to supply air or oxygen to the interior of the furnace. Steps (A) and (B) are carried out sequentially in the furnace chamber, wherein neither the batch is changed, nor the furnace is opened. After the end of step (A) is determined, step (B) proceeds right after the pyrolysis or carbonization by supplying air or oxygen. A dosing of liquid or liquefied substances during the pyrolysis is controlled by at least one parameter of post-combustion. Thermal post-combustion is used for two furnace chambers, one operated for pyrolysis or carbonization and the other operated as a combustion chamber.
摘要翻译： 提供了一种用于处理具有以大能量燃烧的有机部分的具有潜在爆炸性的含贵金属材料的回收炉和方法，所述炉包括用于在炉的燃烧室之间交替操作的切换设备：（A）热解或 在包含最大6重量％氧气的气氛中，在保护炉气体下进行碳化，和（B）包括碳的有机部分的氧化燃烧。 炉具有间接加热和控制，其通过传感器确定热解或碳化的结束，并控制切换设施以向炉内供应空气或氧气。 在炉室中依次进行步骤（A）和（B），其中两个批次都不改变，炉子也不打开。 在确定步骤（A）结束后，步骤（B）通过供应空气或氧气在热解或碳化之后立即进行。 在热解期间，液体或液化物质的剂量由后燃烧的至少一个参数控制。 热后燃烧用于两个炉室，一个用于热解或碳化，另一个用作燃烧室。
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公开(公告)号：US20120227643A1
公开(公告)日：2012-09-13
申请号：US13461114
申请日：2012-05-01
申请人： Christian NOWOTTNY , Horst MEYER , Matthias GREHL , Dieter SCHÄFER , Hans-Joachim ALT , Wilhelm GLAB
发明人： Christian NOWOTTNY , Horst MEYER , Matthias GREHL , Dieter SCHÄFER , Hans-Joachim ALT , Wilhelm GLAB
CPC分类号： C22B7/001 , C22B11/021 , F23G5/0273 , F23G5/16 , F23G5/50 , F23G7/006 , F23G2207/102 , F23G2207/30 , F23G2208/10 , F23G2209/141 , Y02P10/214
摘要： A recycling furnace is provided for processing potentially explosive precious metal-containing materials having organic fractions that combust with great energy. The furnace includes a switching facility for alternating operation of two burning-off chambers of the furnace between: (A) pyrolysis or carbonization under protective furnace gas in an atmosphere comprising maximally 6 wt-% oxygen, and (B) oxidative combustion of the organic fractions including carbon. The furnace has indirect heating and a control that determines the end of the pyrolysis or carbonization by a sensor and controls the switching facility to supply air or oxygen to the interior of the furnace. A continuous conveyor for dosing of liquids or liquefied substances during the pyrolysis is controlled by at least one parameter of post-combustion, preferably a temperature sensor. A single waste gas treatment facility is used for thermal post-combustion for the two furnace chambers.
摘要翻译： 提供回收炉用于处理具有以大能量燃烧的有机部分的具有潜在爆炸性的含贵金属的材料。 炉子包括用于在炉子的两个燃烧室的交替操作的切换设备：（A）在包含最大6重量％的氧的气氛中的保护炉气体下的热解或碳化，和（B）有机物的氧化燃烧 馏分包括碳。 炉具有间接加热和控制，其通过传感器确定热解或碳化的结束，并控制切换设施以向炉内供应空气或氧气。 在热解期间用于计量液体或液化物质的连续输送机由后燃烧，优选温度传感器的至少一个参数控制。 单个废气处理设备用于两个炉室的热后燃烧。
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