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    Silicate luminescent material and its preparation method
    2.
    发明授权
    Silicate luminescent material and its preparation method 有权
    硅酸盐发光材料及其制备方法

    公开(公告)号：US08980131B2

    公开(公告)日：2015-03-17

    申请号：US13512287

    申请日：2009-11-28

    申请人： Mingjie Zhou ,  Chaopu Shi ,  Rong Wang ,  Wenbo Ma

    发明人： Mingjie Zhou ,  Chaopu Shi ,  Rong Wang ,  Wenbo Ma

    IPC分类号： C09K11/66 ,  C09K11/62 ,  C09K11/59

    CPC分类号： C09K11/595

    摘要： Silicate luminescent material and preparation method thereof are provided. The structural formula of the silicate luminescent material is Zn2-y(Si1-xMx)O4:Mny, wherein M is metal element and its oxide is conductive, x is in a range of 0.001 to 0.15, and y is in a range of 0.001 to 0.05. For integrated with conductive metal oxide component, the silicate luminescent material could take advantage of its conductive properties, and the silicate luminescent material could improve the luminescence properties under cathode ray significantly comparing with that of the luminescent material has not been integrated with conductive component. Accordingly, the luminescence efficiency of the above silicate luminescent material is increased.

    摘要翻译： 提供了硅酸盐发光材料及其制备方法。 硅酸盐发光材料的结构式是Zn2-y（Si1-xMx）O4：Mny，其中M是金属元素，其氧化物导电，x在0.001至0.15的范围内，y在0.001的范围内 至0.05。 为了与导电金属氧化物组分集成，硅酸盐发光材料可以利用其导电性能，并且硅酸盐发光材料可以改善阴极射线下的发光特性，与发光材料的发光性能相比，导电组分未被整合。 因此，上述硅酸盐发光材料的发光效率提高。

    METAL NANO PARTICLES DOPED WITH SILICATE LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF
    4.
    发明申请
    METAL NANO PARTICLES DOPED WITH SILICATE LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
    金属纳米颗粒与硅酸盐发光材料及其制备方法

    公开(公告)号：US20130126785A1

    公开(公告)日：2013-05-23

    申请号：US13812908

    申请日：2010-07-30

    申请人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    发明人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    IPC分类号： C09K11/87 ,  C09K11/77

    CPC分类号： C09K11/87 ,  C09K11/7734

    摘要： Metal nano particles doped with silicate luminescent materials and preparation methods thereof are provided. The luminescent materials are represented by the general formula: (Sr1-x-yAxEuy)3SiO5:Dz@Mn, wherein A is one or two selected from alkaline-earth metal elements, D is F or Cl, @ is for coating, M is one or two selected from Ag, Au, Pt, Pd or Cu metal nano particles, 0≦x≦0.5, 0.001

    摘要翻译： 提供掺杂有硅酸盐发光材料的金属纳米颗粒及其制备方法。 发光材料由以下通式表示：（Sr1-x-yAxEuy）3SiO5：Dz @ Mn，其中A为选自碱土金属元素中的一种或两种，D为F或Cl，@为涂层，M为 一种或两种选自Ag，Au，Pt，Pd或Cu金属纳米颗粒，0 @ x @ 0.5，0.001

    ZINC MANGANESE SILICATE CONTAINING METAL PARTICLES LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF
    5.
    发明申请
    ZINC MANGANESE SILICATE CONTAINING METAL PARTICLES LUMINESCENT MATERIALS AND PREPARATION METHODS THEREOF 有权
    包含金属颗粒的金属硅酸盐材料及其制备方法

    公开(公告)号：US20130126784A1

    公开(公告)日：2013-05-23

    申请号：US13703342

    申请日：2010-06-30

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    IPC分类号： C09K11/59 ,  C09K11/87

    CPC分类号： C09K11/59 ,  C01B33/20 ,  C09K11/595 ,  C09K11/87 ,  C09K11/876

    摘要： Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof are provided. The said luminescent materials are represented by the general formula: Zn2-xSiO4: Mnx, My, wherein M is metal, 0.001≦x≦0.1, 0.00001≦y≦0.01. The said methods include the following steps: step 1, preparing silica aerogel containing metal particles; step 2, weighing source compound of zinc, source compound of manganese and the silica aerogel in step 1 at stoichiometric ratio and mixing them to form mixture; step 3, sintering the mixture in step 2, then cooling and grinding to form the said luminescent materials with higher luminescent intensity. The said methods have simple steps, easy operation, low sintering temperature and low cost.

    摘要翻译： 提供了含有金属锰酸锰的发光材料及其制备方法。 所述发光材料由以下通式表示：Zn2-xSiO4：Mnx，My，其中M是金属，0.001 @ x @ 0.1,0.00001 @ y @ 0.01。 所述方法包括以下步骤：步骤1，制备含有金属颗粒的二氧化硅气凝胶; 步骤2，在化学计量比下，在步骤1中称量锌源，锰源和二氧化硅气凝胶，混合形成混合物; 步骤3，在步骤2中烧结混合物，然后冷却和研磨以形成具有较高发光强度的所述发光材料。 所述方法操作简单，操作简便，烧结温度低，成本低。

    Metal nano particles doped with silicate luminescent materials and preparation methods thereof
    7.
    发明授权
    Metal nano particles doped with silicate luminescent materials and preparation methods thereof 有权
    掺有硅酸盐发光材料的金属纳米颗粒及其制备方法

    公开(公告)号：US09206353B2

    公开(公告)日：2015-12-08

    申请号：US13812908

    申请日：2010-07-30

    申请人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    发明人： Mingjie Zhou ,  Rong Wang ,  Chaopu Shi ,  Wenbo Ma

    IPC分类号： C09K11/00 ,  C09K11/87 ,  C09K11/77

    CPC分类号： C09K11/87 ,  C09K11/7734

    摘要： Metal nano particles doped with silicate luminescent materials and preparation methods thereof are provided. The luminescent materials are represented by the general formula: (Sr1-x-yAxEuy)3SiO5:Dz@Mn, wherein A is one or two selected from alkaline-earth metal elements, D is F or Cl, @ is for coating, M is one or two selected from Ag, Au, Pt, Pd or Cu metal nano particles, 0≦x≦0.5, 0.001

    摘要翻译： 提供掺杂有硅酸盐发光材料的金属纳米颗粒及其制备方法。 发光材料由以下通式表示：（Sr1-x-yAxEuy）3SiO5：Dz @ Mn，其中A为选自碱土金属元素中的一种或两种，D为F或Cl，@为涂层，M为 一种或两种选自Ag，Au，Pt，Pd或Cu金属纳米颗粒，0＆lt; lE; x＆lt; lE; 0.5,0.001＆lt; y＆nlE; 0.15和0＆amp; nlE; z＆nlE; 0.5。 n是金属纳米颗粒与硅元素的摩尔比，其中0

    Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof
    8.
    发明授权
    Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof 有权
    含锌锰酸锰的金属颗粒发光材料及其制备方法

    公开(公告)号：US09115309B2

    公开(公告)日：2015-08-25

    申请号：US13703342

    申请日：2010-06-30

    申请人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    发明人： Mingjie Zhou ,  Wenbo Ma ,  Chaopu Shi

    IPC分类号： C09K11/59 ,  C09K11/87 ,  C01B33/20

    CPC分类号： C09K11/59 ,  C01B33/20 ,  C09K11/595 ,  C09K11/87 ,  C09K11/876

    摘要： Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof are provided. The said luminescent materials are a blend of metal M nanoparticles and Zn2-xSiO4:Mnx, wherein M is one of Ag, Au and Pt, 0.001≦x≦0.1, 0.00001≦y≦0.01, y is the molar ratio of M to Zn2-xSiO4:Mnx. The said methods include the following steps: step 1, preparing silica aerogel containing metal particles; step 2, weighing source compound of zinc, source compound of manganese and the silica aerogel in step 1 at stoichiometric ratio and mixing them to form mixture; step 3, sintering the mixture in step 2, then cooling and grinding to form the said luminescent materials with higher luminescent intensity. The said methods have simple steps, easy operation, low sintering temperature and low cost.

    摘要翻译： 提供了含有金属锰酸锰的发光材料及其制备方法。 所述发光材料是金属M纳米颗粒和Zn2-xSiO4：Mnx的共混物，其中M是Ag，Au和Pt之一，0.001和n1E; x和nlE; 0.1,0.00001＆amp; nlE; y＆nlE; 0.01，y是M 到Zn2-xSiO4：Mnx。 所述方法包括以下步骤：步骤1，制备含有金属颗粒的二氧化硅气凝胶; 步骤2，在化学计量比下，在步骤1中称量锌源，锰源和二氧化硅气凝胶，混合形成混合物; 步骤3，在步骤2中烧结混合物，然后冷却和研磨以形成具有较高发光强度的所述发光材料。 所述方法操作简单，操作简便，烧结温度低，成本低。