CLEANING PROCESS THAT PRECIPITATES YTTRIUM OXY-FLOURIDE

    公开(公告)号:US20170282221A1

    公开(公告)日:2017-10-05

    申请号:US15089212

    申请日:2016-04-01

    IPC分类号: B08B3/12 H01J37/32

    摘要: A method includes immersing an article comprising a yttrium based oxide in an acidic cleaning solution comprising water and 1-10 mol % HF acid. A portion of the yttrium based oxide is dissolved by the HF acid. A yttrium based oxy-fluoride is formed based on a reaction between the HF acid and the dissolved portion of the yttrium based. The yttrium based oxy-fluoride is precipitated onto the article over the yttrium based oxide to form a yttrium based oxy-fluoride coating. The acidic cleaning solution may include a yttrium based salt, which may additionally react with the HF acid to form more of the yttrium based oxy-fluoride.

    PLASMA RESISTANT COATING WITH TAILORABLE COEFFICIENT OF THERMAL EXPANSION

    公开(公告)号:US20170260616A1

    公开(公告)日:2017-09-14

    申请号:US15418598

    申请日:2017-01-27

    IPC分类号: C23C4/134 C23C4/04

    CPC分类号: C23C4/134 C23C4/04

    摘要: An article comprises a body and at least one final plasma resistant coating layer on at least one surface of the body. The at least one final plasma resistant coating layer is a mixture of a ScF3 and an initial plasma resistant coating material selected from the group consisting of YF3, Y2O3, a compound of Y4Al2O9, a solid-solution of Y2O3—ZrO2, CaF2, MgF2, SrF2, AlF3, ErF3, LaF3, NdF3, ScF3, CeF4, ZrF4, and combinations thereof. The at least one final plasma resistant coating layer has a thermal expansion coefficient that is within about 20% of the thermal expansion coefficient of the body.