发明申请
- 专利标题: METHOD FOR MANUFACTURING SUCCINIC ACID ESTERS
- 专利标题(中): 制备酸性酯的方法
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申请号: US14767021申请日: 2014-02-13
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公开(公告)号: US20150368170A1公开(公告)日: 2015-12-24
- 发明人: Jan VAN KRIEKEN , André Banier DE HAAN , Jan VAN BREUGEL
- 申请人: PURAC BIOCHEM BV
- 优先权: EP13155241.6 20130214
- 国际申请: PCT/EP2014/052825 WO 20140213
- 主分类号: C07C29/09
- IPC分类号: C07C29/09 ; C07C67/08
摘要:
The invention pertains to a process for preparing a succinic acid ester comprising the steps of bringing an aqueous liquid comprising succinic acid, alcohol, and at least 5 wt. % of a dissolved chloride salt selected from magnesium chloride, calcium chloride, and zinc chloride, calculated on the weight of the liquid, to reaction conditions, thereby obtaining a succinic acid ester, and recovering the succinic acid ester and an aqueous solution comprising the dissolved chloride salt. It has been found that the process according to the invention shows a high yield and has a high reaction rate. Additionally, it has been found that the process makes it possible to carry out the separation of the succinic acid ester from the aqueous reaction medium in high yield.
公开/授权文献
- US09249073B2 Method for manufacturing succinic acid esters 公开/授权日:2016-02-02
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