- 专利标题: Method for preparing the nano-porous oxide-noble metal composite material by deoxidation
-
申请号: US15626127申请日: 2017-06-18
-
公开(公告)号: US10183278B2公开(公告)日: 2019-01-22
- 发明人: Guijing Li , Wenjie Feng , Jinxi Liu , Xueqian Fang
- 申请人: SHIJIAZHUANG TIEDAO UNIVERSITY
- 代理机构: W&K IP
- 优先权: CN201710124757 20170303
- 主分类号: B01J21/02
- IPC分类号: B01J21/02 ; B01J21/06 ; B01J23/10 ; B01J23/38 ; B01J23/42 ; B01J23/44 ; B01J23/50 ; B01J23/52 ; B01J23/54 ; B01J23/56 ; B01J23/63 ; B01J23/66 ; B01J23/72 ; B01J23/745 ; B01J23/83 ; B01J23/89 ; B01J37/02 ; B01J35/00 ; B01J35/10
摘要:
The present invention discloses a method for preparing the nano-porous oxide-noble metal composite material by deoxidation, comprising dissolving the noble metal ion or fine particles, the oxide salt to be dissolved and the target oxide salt in the pure water in a proportion to form the mixed solution, adding the surface active agent, and stirring magnetically; dropping the precipitant gradually to form the precipitate, stirring for 4 h, separating and cleaning the precipitate, and drying, grinding and calcining at a high temperature; corroding fully and dissolving part of the oxide with an etchant, preserving the noble metal and the target oxide, separating, cleaning, drying at 80° C., and heat treating at a high temperature to obtain the nano-porous oxide-noble metal composite material. The present invention has the technological advantages of simple operation, low energy consumption, environmental protection and suitable for batching, etc.
公开/授权文献
信息查询