METHOD FOR PRODUCING ZIRCONIA SINTERED BODY
    7.
    发明公开

    公开(公告)号:US20230382808A1

    公开(公告)日:2023-11-30

    申请号:US18027680

    申请日:2021-09-24

    Inventor: Atsushi MATSUURA

    Abstract: The present invention provides a method of production of a zirconia sintered body by which a zirconia molded body or zirconia pre-sintered body having a plurality of layers containing different amounts of stabilizer is sintered in a short time period to produce a zirconia sintered body having hardly noticeable stripes between layers differing in yttria content. The present invention relates to a method for producing a zirconia sintered body, comprising a firing step of firing a zirconia molded body or a zirconia pre-sintered body,



    the zirconia molded body or the zirconia pre-sintered body comprising a plurality of layers containing a stabilizer,
    the plurality of layers including layers having different stabilizer contents,
    the firing step comprising at least three stages of temperature-increasing process including a first temperature-increasing step (H1), a second temperature-increasing step (H2), and a third temperature-increasing step (H3),
    the method satisfying HR2=more than 0° C./min and less than 50° C./min, HR3=5 to 150° C./min, and HR3/HR2>1, where HR2 is a rate of temperature increase in H2, and HR3 is a rate of temperature increase in H3,
    the temperature-increasing process having start temperatures that are 1,000° C. or less in H1, more than 1,250° C. and 1,450° C. or less in H2, and 1,450° C. or more and 1,550° C. or less in H3,
    the temperature-increasing process having end temperatures that are more than 1,250° C. and 1,450° C. or less in H1, 1,450° C. or more and 1,550° C. or less in H2, and 1,500° C. or more and 1,750° C. or less in H3.

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