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    METHOD FOR THE MANUFACTURE OF BISPHENOL A
    1.
    发明公开
    METHOD FOR THE MANUFACTURE OF BISPHENOL A 审中-公开

    公开(公告)号：US20240308944A1

    公开(公告)日：2024-09-19

    申请号：US18576586

    申请日：2022-06-13

    Applicant: SABIC Global Technologies B.V.

    Inventor： Surya Prakasa Rao Daliparthi ,  Paulus Johannes Maria Eijsbouts ,  Gert-Jan Schoenmakers

    IPC: C07C37/84 ,  B01J14/00 ,  B01J31/08 ,  C07C37/74

    CPC classification number: C07C37/84 ,  B01J14/005 ,  B01J31/08 ,  C07C37/74 ,  B01J2219/00033 ,  C07C2601/16

    Abstract: A method for the continuous manufacture of bisphenol A comprising i) feeding one or more feed streams comprising phenol and acetone to a reactor and reacting said acetone and phenol in the presence of an ion-exchange resin catalyst thereby forming a product stream comprising bisphenol A, phenol, acetone, water and by-products, ii) crystallising bisphenol A and/or bisphenol A/phenol adduct crystals from said product stream in one or more crystallisation units thereby forming a slurry consisting of said crystals and a mother liquor, iii) separating the mother liquor from the crystals in one or more solid-liquid separation units, iv) heating the mother liquor in a heat recovery unit and feeding the heated mother liquor to a distillation column, v) separating the mother liquor in the distillation column thereby forming a bottom stream comprising phenol and a top stream comprising water, vi) cooling the bottom stream in said heat recovery unit.

    EXTENDED RESIDENCE TIME CENTRIFUGAL CONTACTOR DESIGN MODIFICATION AND CENTRIFUGAL CONTACTOR VANE PLATE VALVING APPARATUS FOR EXTENDING MIXING ZONE RESIDENCE TIME
    4.
    发明申请
    EXTENDED RESIDENCE TIME CENTRIFUGAL CONTACTOR DESIGN MODIFICATION AND CENTRIFUGAL CONTACTOR VANE PLATE VALVING APPARATUS FOR EXTENDING MIXING ZONE RESIDENCE TIME 有权
    扩展住宅时间离心式接触器设计修改和离心式接触器叶片式阀门设备，用于扩展混合区居住时间

    公开(公告)号：US20160089617A1

    公开(公告)日：2016-03-31

    申请号：US14501898

    申请日：2014-09-30

    Applicant: UCHICAGO ARGONNE, LLC

    Inventor： Kent E. Wardle

    IPC: B01D11/04 ,  B01J19/18 ,  B01D15/18

    CPC classification number: B01D11/048 ,  B01D15/1807 ,  B01D2011/002 ,  B01J14/005 ,  B01J19/18 ,  B01J2219/00024 ,  B01J2219/00094 ,  B01J2219/185

    Abstract: The present invention provides an annular centrifugal contactor, having a housing adapted to receive a plurality of flowing liquids; a rotor on the interior of the housing; an annular mixing zone, wherein the annular mixing zone has a plurality of fluid retention reservoirs with ingress apertures near the bottom of the annular mixing zone and egress apertures located above the ingress apertures of the annular mixing zone; and an adjustable vane plate stem, wherein the stem can be raised to restrict the flow of a liquid into the rotor or lowered to increase the flow of the liquid into the rotor.

    Abstract translation: 本发明提供了一种环形离心接触器，其具有适于容纳多个流动液体的壳体; 壳体内部的转子; 环形混合区，其中所述环形混合区具有多个流体保留储存器，所述流体保留储存器具有靠近所述环形混合区的底部的入口孔和位于所述环形混合区的入口孔的上方的出口孔; 以及可调叶片板杆，其中可以升高杆以限制液体进入转子的流动或降低以增加液体进入转子的流动。

    Hydrophilic membrane integrated olefin hydration process
    5.
    发明授权
    Hydrophilic membrane integrated olefin hydration process 有权
    亲水膜整合烯烃水合过程

    公开(公告)号：US09199214B2

    公开(公告)日：2015-12-01

    申请号：US14516851

    申请日：2014-10-17

    Applicant: Saudi Arabian Oil Company

    Inventor： Aadesh Harale ,  Wei Xu ,  Ibrahim Abba

    IPC: C07C29/04 ,  C07C29/74 ,  C07C29/76 ,  B01J14/00 ,  B01J19/00 ,  B01J8/04 ,  B01J8/00 ,  C07C29/17

    CPC classification number: B01J14/00 ,  B01J8/009 ,  B01J8/0453 ,  B01J8/0492 ,  B01J14/005 ,  B01J19/0053 ,  C07C29/04 ,  C07C29/172 ,  C07C29/74 ,  C07C29/76 ,  Y02P20/582 ,  C07C31/12

    Abstract: A membrane-integrated hydration reactor that is operable to produce an associated alcohol product from an olefin using water includes a solid acid olefin hydration catalyst in a production zone and a hydrophilic membrane operable to selectively permit pervaporation of water one-way and not permit pervaporation of the associated alcohol or permeation of the olefin at olefin hydration process conditions in a separations zone. The production zone is operable to form a production zone product mixture made of the associated alcohol and any unreacted water. The associated separations zone is operable to form and produce both the associated alcohol product and a pervaporated water product from the production zone product mixture. A method of olefin hydration for forming an associated alcohol product from an olefin using water uses the membrane-integrated hydration reactor at olefin hydration process conditions.

    Abstract translation: 可用于使用水从烯烃生产相关的醇产物的膜整合的水合反应器包括在生产区中的固体酸性烯烃水合催化剂和可操作以选择性地允许单向渗透蒸发的亲水膜，并且不允许渗透蒸发 相关的醇或烯烃在分离区中的烯烃水合过程条件下的渗透。 生产区可操作地形成由相关的醇和任何未反应的水制成的生产区产品混合物。 相关联的分离区域可操作以从生产区产品混合物形成和产生相关联的醇产物和蒸发水产物。 使用水从烯烃形成相关的醇产物的烯烃水合方法在烯烃水合工艺条件下使用膜一体​​化水合反应器。

    Apparatus and method of reacting polymers passing through metal ion chelated resin matrix to produce injectable medical devices
    6.
    发明授权
    Apparatus and method of reacting polymers passing through metal ion chelated resin matrix to produce injectable medical devices 有权
    使通过金属离子螯合树脂基质的聚合物反应产生可注射医疗器械的装置和方法

    公开(公告)号：US09039979B2

    公开(公告)日：2015-05-26

    申请号：US13202348

    申请日：2010-02-22

    Applicant: Sébastien Ladet ,  Philippe Gravagna

    Inventor： Sébastien Ladet ,  Philippe Gravagna

    IPC: B01J19/18 ,  B01J19/00 ,  B01J14/00 ,  A61B17/00 ,  B01F5/06 ,  B01F13/00 ,  B01J23/72 ,  B01J35/04

    CPC classification number: B01J19/18 ,  A61B17/00491 ,  A61B2017/00495 ,  B01F5/0615 ,  B01F5/0683 ,  B01F5/0688 ,  B01F13/002 ,  B01F13/0023 ,  B01J14/005 ,  B01J19/0053 ,  B01J19/0066 ,  B01J23/72 ,  B01J35/04 ,  B01J2219/00761 ,  C08G63/66

    Abstract: The present disclosure relates to an apparatus and process for forming medical devices from an injectable composition. The apparatus includes a supply assembly configured to maintain and selective dispense a first precursor and a second precursor, a mixing assembly configured to mix the first and second precursors, and at least one catalyzing element including a transition metal ion to aid in the polymerization of the first and second precursors. The process includes dispensing a volume of the first precursor and a volume of the second precursor into a mixing assembly and mixing the first and second precursors. The first and second precursors each possess a core and at least one functional group known to have click reactivity with each other. The mixed precursors are contacted with a transition metal catalyst to produce a flowable composition for use as a medical device.

    Abstract translation: 本公开涉及一种用于从可注射组合物形成医疗装置的装置和方法。 该设备包括供应组件，其被配置为维持和选择性地分配第一前体和第二前体，配置成混合第一和第二前体的混合组件和包含过渡金属离子的至少一个催化元素以有助于聚合 第一和第二前体。 该方法包括将体积的第一前体和体积的第二前体分配到混合组件中并混合第一和第二前体。 第一和第二前体各自具有核心和至少一个已知具有彼此具有点击反应性的官能团。 混合的前体与过渡金属催化剂接触以产生用作医疗装置的可流动组合物。

    CATALYTIC STATIC MIXING REACTOR
    8.
    发明申请
    CATALYTIC STATIC MIXING REACTOR 审中-公开
    催化稳态反应器

    公开(公告)号：US20140072481A1

    公开(公告)日：2014-03-13

    申请号：US13613555

    申请日：2012-09-13

    Applicant: John Scahill

    Inventor： John Scahill

    IPC: B01J19/24

    CPC classification number: B01F5/0615 ,  B01D53/88 ,  B01F5/0473 ,  B01J14/005 ,  B01J15/005 ,  B01J19/006 ,  B01J19/0066 ,  B01J19/2415 ,  B01J19/2445 ,  B01J2219/00024 ,  B01J2219/00094

    Abstract: A catalytic static mixing reactor has a conduit casing defined about an axis of a fluid flow. A catalyst is deposited on a mixing element. The mixing element is adapted to be inserted in the conduit. The element provides an exceptionally high surface area and is formed to obstacle the primary flow inducing a first order mixing phenomenon. The element is formed with at least one irregular surface or edge capable of inducing a second order mixing phenomenon. The irregular surface is adapted as a catalytic supporting surface. The supporting surface supports the deposition of the catalyst thereon so that a third order chemical reaction phenomenon is coupled with that of said first and second order mixing phenomenon at the catalytic surface so that a reactant to be converted in the fluid flow is converted to at least one predetermined product during said first and second order mixing phenomenon.

    Abstract translation: 催化静态混合反应器具有围绕流体流动轴线限定的导管壳体。 催化剂沉积在混合元件上。 混合元件适于插入导管中。 该元件提供了非常高的表面积，并形成为阻碍主流引起一阶混合现象。 该元件形成有能够引起二阶混合现象的至少一个不规则表面或边缘。 不规则表面适合作为催化支撑表面。 支撑表面支持催化剂在其上的沉积，使得三级化学反应现象与在催化表面处的所述第一和第二阶混合现象的偶联现象相结合，使得要在流体流中转化的反应物转化为至少 在所述第一和第二阶混合现象期间一个预定的产品。

    ENHANCEMENT OF SURFACE-ACTIVE SOLID-PHASE HETEROGENEOUS CATALYSTS
    9.
    发明申请
    ENHANCEMENT OF SURFACE-ACTIVE SOLID-PHASE HETEROGENEOUS CATALYSTS 有权
    表面活性固体相异构催化剂的增强

    公开(公告)号：US20120197056A1

    公开(公告)日：2012-08-02

    申请号：US13219293

    申请日：2011-08-26

    Applicant: Mitchell A. Cotter

    Inventor： Mitchell A. Cotter

    IPC: C07C2/76 ,  B01J8/18 ,  B32B3/02 ,  B01J19/00

    CPC classification number: B01J35/026 ,  B01J8/0095 ,  B01J8/02 ,  B01J8/22 ,  B01J8/222 ,  B01J8/24 ,  B01J10/007 ,  B01J12/007 ,  B01J14/005 ,  B01J15/005 ,  B01J16/005 ,  B01J19/18 ,  B01J19/1812 ,  B01J19/20 ,  B01J19/26 ,  B01J19/30 ,  B01J23/44 ,  B01J35/023 ,  B01J37/0225 ,  B01J2208/00672 ,  B01J2219/30234 ,  B01J2219/30246 ,  B01J2219/30296 ,  B01J2219/30408 ,  B01J2219/30416 ,  B01J2219/30475 ,  F04C2/084 ,  F04C2/10 ,  F04C2/18 ,  F04C13/00 ,  Y10T428/16

    Abstract: Surface-active solid-phase catalyst activity may be substantially improved by creating deliberate repetitive surface-to-surface contact between portions of the active surfaces of catalyst objects. While they are immersed in reactant material such contact between portions of the active surfaces of catalyst objects can substantially activate the surfaces of many heterogeneous catalysts. Examples are given of such action employing a multitude of predetermined shapes, supported catalyst structures, etc. agitated or otherwise brought into contact to produce numerous surface collisions. One embodiment employs a gear pump mechanism with catalytically active-surfaced gear teeth to create the repetitive transient contacting action during pumping of a flow of reactant. The invention is applicable to many other forms for creating transient catalytic surface contacting action. Optionally catalytic output of such systems may be significantly further improved by employing radiant energy or vibration.

    Abstract translation: 通过在催化剂物体的活性表面的部分之间产生有意义的重复的表面 - 表面接触，可以显着改善表面活性固相催化剂活性。 当它们浸入反应物材料中时，催化剂物体的活性表面的部分之间的接触可基本上活化许多非均相催化剂的表面。 给出了使用多种预定形状，负载催化剂结构等的这种动作的实例，其被搅动或以其它方式接触以产生许多表面碰撞。 一个实施例采用具有催化活性表面齿轮齿的齿轮泵机构，以在泵送反应物流期间产生重复的瞬时接触作用。 本发明可应用于许多其它用于产生瞬时催化表面接触作用的形式。 可以通过采用辐射能或振动来显着进一步改进这种系统的催化输出。

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