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    Thin film for anode of lithium secondary battery and manufacturing method thereof
    33.
    发明授权
    Thin film for anode of lithium secondary battery and manufacturing method thereof 有权
    锂二次电池用阳极用薄膜及其制造方法

    公开(公告)号：US06824922B2

    公开(公告)日：2004-11-30

    申请号：US10118030

    申请日：2002-04-09

    Applicant: Young-sin Park ,  Joo-yeal Oh ,  Hong-koo Baik ,  Sung-man Lee

    Inventor： Young-sin Park ,  Joo-yeal Oh ,  Hong-koo Baik ,  Sung-man Lee

    IPC: H01M438

    CPC classification number: H01M10/0436 ,  H01M4/134 ,  H01M4/1391 ,  H01M4/1397 ,  H01M4/366 ,  H01M4/38 ,  H01M4/386 ,  H01M4/525 ,  H01M4/54 ,  H01M10/052 ,  H01M10/0562 ,  H01M2004/027

    Abstract: A thin film for an anode of a lithium secondary battery having a current collector and an anode active material layer formed thereon is provided. The anode active material layer is a multi-layered thin film formed by stacking a silver (Ag) layer and a silicon-metal (Si-M) layer having silicon dispersed in a base made from metal reacting with silicon while not reacting with lithium. The cycle characteristic of the thin film for an anode can be improved by suppressing the volumetric expansion and shrinkage of Si occurring during charging/discharging cycles. Thus, a lithium secondary battery with improved life characteristics by employing the thin film for an anode, which greatly improves the chemical, mechanical stability of the interface between an electrode and an electrolyte.

    Abstract translation: 提供一种用于形成有集电体和负极活性物质层的锂二次电池的负极的薄膜。 负极活性物质层是通过层叠银（Ag）层和分散在由与金反应的金属制成的基体中的硅的硅 - 金属（Si-M）层而不与锂反应而形成的多层薄膜。 通过抑制在充放电循环中发生的Si的体积膨胀和收缩，可以提高阳极用薄膜的循环特性。 因此，通过使用用于阳极的薄膜来改善寿命特性的锂二次电池，其极大地改善了电极和电解质之间的界面的化学，机械稳定性。

    Diffusion barrier layer for semiconductor device and fabrication method thereof
    34.
    发明授权
    Diffusion barrier layer for semiconductor device and fabrication method thereof 有权
    半导体器件用扩散阻挡层及其制造方法

    公开(公告)号：US06482734B1

    公开(公告)日：2002-11-19

    申请号：US09233040

    申请日：1999-01-20

    Applicant: Jae-Hee Ha ,  Hong Koo Baik ,  Sung-Man Lee

    Inventor： Jae-Hee Ha ,  Hong Koo Baik ,  Sung-Man Lee

    IPC: H01L214763

    CPC classification number: H01L21/76864 ,  H01L21/28568 ,  H01L21/31604 ,  H01L21/76843 ,  H01L23/485 ,  H01L2924/0002 ,  H01L2924/00

    Abstract: The present invention relates to a diffusion barrier layer for a semiconductor device and fabrication method thereof. The diffusion barrier layer according to the present invention is fabricated by forming a diffusion barrier layer containing a refractory metal material and an insulating material on an insulating layer and in a contact hole, wherein the insulating layer being partially etched to form the contact hole, is formed on a semiconductor substrate; and annealing the diffusion barrier layer. Therefore, an object of the present invention is to provide a diffusion barrier layer for a semiconductor device, which is of an amorphous or microcrystalline state and thermodynamically stable even at a high temperature since an insulating material is bonded to a refractory metal material in the diffusion barrier layer.

    Abstract translation: 本发明涉及一种用于半导体器件的扩散阻挡层及其制造方法。 根据本发明的扩散阻挡层通过在绝缘层和接触孔中形成包含难熔金属材料和绝缘材料的扩散阻挡层来制造，其中部分蚀刻以形成接触孔的绝缘层是 形成在半导体衬底上; 和退火扩散阻挡层。 因此，本发明的目的是提供一种半导体器件的扩散阻挡层，该扩散阻挡层具有非晶态或微晶态，并且即使在高温下也具有热力学稳定性，因为绝缘材料与扩散中的难熔金属材料结合 阻挡层。

    NEGATIVE ACTIVE MATERIAL FOR LITHIUM SECONDARY BATTERY AND A METHOD FOR PREPARING SAME
    36.
    发明申请
    NEGATIVE ACTIVE MATERIAL FOR LITHIUM SECONDARY BATTERY AND A METHOD FOR PREPARING SAME 有权
    用于锂二次电池的负极活性材料及其制备方法

    公开(公告)号：US20110175020A1

    公开(公告)日：2011-07-21

    申请号：US13020305

    申请日：2011-02-03

    Applicant: Sung-Man LEE ,  Heon Young LEE ,  Moon Ki HONG

    Inventor： Sung-Man LEE ,  Heon Young LEE ,  Moon Ki HONG

    IPC: H01M4/86

    CPC classification number: H01M4/1395 ,  H01M4/02 ,  H01M4/0471 ,  H01M4/049 ,  H01M4/13 ,  H01M4/131 ,  H01M4/133 ,  H01M4/134 ,  H01M4/139 ,  H01M4/366 ,  H01M4/386 ,  H01M4/48 ,  H01M4/485 ,  H01M4/625 ,  H01M10/0525 ,  Y02E60/122

    Abstract: Provided are an anode active material for a lithium secondary battery having high reversible capacity and excellent charge/discharge efficiency, comprising a complex composed of ultra-fine Si phase particles and an oxide surrounding the ultra-fine Si phase particles, and a carbon material; and a method for preparing the same. The present invention also provides a method for preparing an anode active material for a lithium secondary battery comprising producing a complex composed of ultra-fine Si particles and an oxide surrounding the ultra-fine Si particles by mixing a silicon oxide and a material having an absolute value of oxide formation enthalpy (ΔHfor)greater than that of the silicon oxide and negative oxide formation enthalpy by a mechanochemical process or subjecting them to a thermochemical reaction to reduce the silicon oxide; and mixing the Si phase-containing oxide complex and carbon material.

    Abstract translation: 本发明提供一种锂二次电池的负极活性物质，其具有高的可逆容量和优异的充放电效率，包括由超细Si相颗粒和围绕超细Si相颗粒的氧化物组成的复合体和碳材料; 及其制备方法。 本发明还提供一种锂二次电池用负极活性物质的制造方法，其特征在于，通过混合氧化硅和绝缘材料，制造由超细Si粒子和超细Si粒子构成的氧化物构成的络合物 通过机械化学方法氧化物形成焓（＆Dgr; Hfor）的值大于氧化硅的值和负氧化物形成焓，或使其进行热化学反应以还原氧化硅; 并混合含Si相的氧化物络合物和碳材料。

    Anode active material for lithium secondary battery and a method for preparing the same
    37.
    发明授权
    Anode active material for lithium secondary battery and a method for preparing the same 有权
    锂二次电池用阳极活性物质及其制备方法

    公开(公告)号：US07906236B2

    公开(公告)日：2011-03-15

    申请号：US10566344

    申请日：2004-07-29

    Applicant: Sung-Man Lee ,  Heon Young Lee ,  Moon Ki Hong

    Inventor： Sung-Man Lee ,  Heon Young Lee ,  Moon Ki Hong

    IPC: H01M4/58

    CPC classification number: H01M4/1395 ,  H01M4/02 ,  H01M4/0471 ,  H01M4/049 ,  H01M4/13 ,  H01M4/131 ,  H01M4/133 ,  H01M4/134 ,  H01M4/139 ,  H01M4/366 ,  H01M4/386 ,  H01M4/48 ,  H01M4/485 ,  H01M4/625 ,  H01M10/0525 ,  Y02E60/122

    Abstract: Provided are an anode active material for a lithium secondary battery having high reversible capacity and excellent charge/discharge efficiency, comprising a complex composed of ultra-fine Si phase particles and an oxide surrounding the ultra-fine Si phase particles, and a carbon material; and a method for preparing the same. The present invention also provides a method for preparing an anode active material for a lithium secondary battery comprising producing a complex composed of ultra-fine Si particles and an oxide surrounding the ultra-fine Si particles by mixing a silicon oxide and a material having an absolute value of oxide formation enthalpy (ΔHfor) greater than that of the silicon oxide and negative oxide formation enthalpy by a mechanochemical process or subjecting them to a thermochemical reaction to reduce the silicon oxide; and mixing the Si phase-containing oxide complex and carbon material.

    Abstract translation: 本发明提供一种锂二次电池的负极活性物质，其具有高的可逆容量和优异的充放电效率，包括由超细Si相颗粒和围绕超细Si相颗粒的氧化物组成的复合体和碳材料; 及其制备方法。 本发明还提供一种锂二次电池用负极活性物质的制造方法，其特征在于，通过混合氧化硅和绝缘材料，制造由超细Si粒子和超细Si粒子构成的氧化物构成的络合物 通过机械化学方法氧化物形成焓（＆Dgr; Hfor）的值大于氧化硅的值和负氧化物形成焓，或使其进行热化学反应以还原氧化硅; 并混合含Si相的氧化物络合物和碳材料。

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