发明授权
US09475790B2 Method for preparing refined lactide from recovered polylactic acid
有权
从回收聚乳酸制备精制丙交酯的方法
- 专利标题: Method for preparing refined lactide from recovered polylactic acid
- 专利标题(中): 从回收聚乳酸制备精制丙交酯的方法
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申请号: US14534151申请日: 2014-11-05
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公开(公告)号: US09475790B2公开(公告)日: 2016-10-25
- 发明人: Yihu Yang , Jie Xu
- 申请人: Xiaogan Esun New Material Co., Ltd.
- 申请人地址: CN Xiaogan
- 专利权人: XIAOGAN ESUN MATERIAL CO., LTD.
- 当前专利权人: XIAOGAN ESUN MATERIAL CO., LTD.
- 当前专利权人地址: CN Xiaogan
- 代理机构: Matthias Scholl, PC
- 代理商 Matthias Scholl
- 主分类号: C07D319/00
- IPC分类号: C07D319/00 ; C07D319/12 ; C08J11/12 ; C08J11/16
摘要:
A method for preparing lactide from recovered polylactic acid, the method including the following steps: A. pretreating the recovered polylactic acid; B. extruding the treated polylactic acid from a twin screw extruder to yield a polylactic acid melt, and introducing the polylactic acid melt to a pre-depolymerization kettle; C. carrying out a chain scission reaction to break molecular chains in the polylactic acid melt and to decrease the number-average molecular weight of the polylactic acid melt to below 5000; D. conducting depolymerization reaction to yield a crude lactide; and E. purifying the crude lactide and crystallizing the purified lactide.
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