Invention Grant
- Patent Title: α,α-difluoroacetaldehyde production method
- Patent Title (中): α,α-二氟乙醛生产方法
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Application No.: US14761774Application Date: 2014-01-23
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Publication No.: US09440900B2Publication Date: 2016-09-13
- Inventor: Takashi Ootsuka , Mari Imamura , Akihiro Ishii , Koji Ueda , Shunsuke Mimura
- Applicant: Central Glass Company, Limited
- Applicant Address: JP Ube-shi
- Assignee: Central Glass Company, Limited
- Current Assignee: Central Glass Company, Limited
- Current Assignee Address: JP Ube-shi
- Agency: Crowell & Moring LLP
- Priority: JP2013-012532 20130125
- International Application: PCT/JP2014/051365 WO 20140123
- International Announcement: WO2014/115801 WO 20140731
- Main IPC: C07C45/41
- IPC: C07C45/41

Abstract:
A production method of α,α-difluoroacetaldehyde according to the present invention includes reaction of an α,α-difluoroacetic acid ester with hydrogen gas (H2) in the presence of a ruthenium catalyst. It is possible to selectively obtain α,α-difluoroacetaldehyde as a partially reduced product of the hydrogenation reaction by the adoption of specific reaction conditions (in particular, reaction solvent and reaction temperature). This hydrogenation process can be alternative to the industrially unpractical hydride reduction process.
Public/Granted literature
- US20150329455A1 Alpha,Alpha-Difluoroacetaldehyde Production Method Public/Granted day:2015-11-19
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