- 专利标题: Method of preparing co-polymer particles
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申请号: US09821034申请日: 2001-03-30
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公开(公告)号: US06528582B2公开(公告)日: 2003-03-04
- 发明人: Kwok Tang , Guomin Bian , Leena Matilainen , Sinikka Ingelin
- 申请人: Kwok Tang , Guomin Bian , Leena Matilainen , Sinikka Ingelin
- 主分类号: C08L6124
- IPC分类号: C08L6124
摘要:
A one-step, in-situ, process for producing a high solids content emulsion or dispersion of partially or totally crosslinked urea formaldehyde (UF), melamine formaldehyde (MF), or melamine urea formaldehyde (MUF) resin droplets or particles, by forming a reaction mixture of (i) aqueous formaldehyde (formalin), (ii) at least one water-soluble protective colloid, (iii) water and (iv) optionally a surfactant, and mixing the reaction mixture in a reaction vessel; optionally adjusting the initial pH of the reaction mixture according to a desired value as needed; adding (i) urea or substituted urea, (ii) melamine or substituted melamine, or (iii) a mixture thereof, to the reaction mixture; and heating the reaction mixture to a temperature at which condensation takes place between the (i) urea or substituted urea, (ii) the melamine or substituted melamine, or (iii) the mixture thereof, and the formaldehyde to form a urea formaldehyde, melamine formaldehyde or melamine urea formaldehyde resin, and holding the reaction mixture at that temperature or a higher temperature, under mixing, for a period of time sufficient to achieve a desired degree of crosslinking in said urea formaldehyde, melamine formaldehyde or melamine urea formaldehyde resin; and cooling the reaction mixture. The droplet or particle size of the resulting resin dispersion can be controlled and adjusted by way of the present technique to the application requirements.
公开/授权文献
- US20020004554A1 Method of preparing co-polymer particles 公开/授权日:2002-01-10
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