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US5376622A Method of manufacturing an ingot of a high critical temperature superconductive oxide 失效
制造高临界温度超导氧化物锭的方法

Method of manufacturing an ingot of a high critical temperature
superconductive oxide
Abstract:
A melting-and-solidification manufacturing method for manufacturing an ingot of a high critical temperature superconductive oxide belonging, in particular, to the YBaCuO, BiSrCaCuO, or TlBaCaCuO families, wherein:an ingot of oxide having the appropriate stoichiometery is used;the ingot is held horizontally by levitation on a film of gas inside a furnace;the ingot is melted;a vertical thermal gradient is established inside said furnace such that nucleation starts at the bottom portion of said ingot;while maintaining said thermal gradient, the overall temperature of the furnace is lowered at a rate of not more than 0.1.degree. C./hour down to the temperature which corresponds to complete ingot solidification; andfinally, conventional oxygenation treatment is applied to said ingot.
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