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US4266981A Process for recovering and utilizing cellulose using sulfuric acid 失效
使用硫酸回收利用纤维素的方法

Process for recovering and utilizing cellulose using sulfuric acid
Abstract:
A process for recovering cellulose using sulfuric acid and utilizing the recovered cellulose by hydrolysis to yield glucose. Cellulosic raw materials are hydrolyzed by dilute sulfuric acid to remove hemicellulose, after which the solid residue is separated and is treated with concentrated sulfuric acid to dissolve cellulose contained therein. After blending and mixing of the residue in the concentrated sulfuric acid under mild reaction conditions, cellulose is reprecipitated by addition of water or an organic solvent such as methanol. The recovered cellulose can then be hydrolyzed by cellulose enzymes and/or dilute acids to provide a high yield of glucose. High level recovery and reconcentration of the sulfuric acid is also disclosed.
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