- 专利标题: METHOD FOR PREPARING A CATALYST COMPRISING A NICKEL ACTIVE PHASE DISTRIBUTED IN A CRUST VIA IMPREGNATION OF HEPTANOL
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申请号: US18576257申请日: 2022-07-12
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公开(公告)号: US20240326032A1公开(公告)日: 2024-10-03
- 发明人: Malika BOUALLEG , Laetitia JOTHIE
- 申请人: IFP ENERGIES NOUVELLES
- 申请人地址: FR RUEIL-MALMAISON
- 专利权人: IFP ENERGIES NOUVELLES
- 当前专利权人: IFP ENERGIES NOUVELLES
- 当前专利权人地址: FR RUEIL-MALMAISON
- 优先权: FR 2107963 2021.07.22
- 国际申请: PCT/EP2022/069500 2022.07.12
- 进入国家日期: 2024-01-03
- 主分类号: B01J37/02
- IPC分类号: B01J37/02 ; B01J21/04 ; B01J23/755 ; B01J35/30 ; B01J37/00 ; B01J37/08 ; B01J37/18 ; C07C5/05 ; C07C5/11
摘要:
Process for preparing a catalyst comprising a nickel active phase and an alumina support, said catalyst comprising between 1% and 50% by weight of elemental nickel relative to the total weight of the catalyst, the nickel being distributed both over a crust at the periphery of the support, and at the core of the support, which process comprises the following steps:
a) said support is impregnated with a volume V1 of a heptanol solution of between 0.2 and 0.8 times the total pore volume TPV of said support in order to obtain an impregnated support;
b) the impregnated support obtained at the end of step a) is impregnated with a solution comprising a precursor of the nickel active phase in order to obtain a catalyst precursor;
c) the catalyst precursor obtained at the end of step b) is dried at a temperature below 250° C.
a) said support is impregnated with a volume V1 of a heptanol solution of between 0.2 and 0.8 times the total pore volume TPV of said support in order to obtain an impregnated support;
b) the impregnated support obtained at the end of step a) is impregnated with a solution comprising a precursor of the nickel active phase in order to obtain a catalyst precursor;
c) the catalyst precursor obtained at the end of step b) is dried at a temperature below 250° C.
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