Invention Publication
- Patent Title: MULTI-STEP PROCESS FOR MAKING CATHODE ACTIVE MATERIALS, AND CATHODE ACTIVE MATERIALS
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Application No.: US18037663Application Date: 2021-11-10
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Publication No.: US20230361294A1Publication Date: 2023-11-09
- Inventor: Heino Sommer , Felix Florian Riewald , Philipp Kurzhals
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Priority: EP 209036.1 2020.11.20
- International Application: PCT/EP2021/081174 2021.11.10
- Date entered country: 2023-05-18
- Main IPC: H01M4/525
- IPC: H01M4/525 ; C01G53/00 ; H01M4/04 ; H01M4/131 ; H01M4/62 ; H01M10/052

Abstract:
The present invention is related to a process for making an electrode active material wherein said process comprises the following steps: (a) Providing a hydroxide TM(OH)2 or at least one oxide TMO or at least one oxyhydroxide of TM or a combination of at least two of the foregoing wherein TM is one or more metals and contains at least 97 mol-% Ni and, optionally, in total up to 3 mol-% of at least one metal selected from Al, Ti, Zr, V, Co, Zn, Ba, and Mn; (b) mixing said hydroxide TM(OH)2 or oxide TMO or oxyhydroxide of TM or combination with a source of lithium and a source of Mg wherein the molar amount of (Li+Mg) corresponds to 75 to 95 mol-% of TM; (c) treating the mixture obtained from step (b) thermally at a temperature in the range of from 450 to 650° C., thereby obtaining an intermediate; (d) mixing the intermediate from step (c) with a source of Li and with at least one compound of a metal M1 selected from Al, Zr, Co, Mn, Nb, Ta, Mo, and W; (e) treating the mixture obtained from step (d) thermally at a temperature in the range of from 500 to 850° C.
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