- 专利标题: METHOD AND DEVICE FOR PREPARING CARBON NANOTUBES AND HYDROGEN
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申请号: US17793719申请日: 2020-12-07
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公开(公告)号: US20230348264A1公开(公告)日: 2023-11-02
- 发明人: Yan LI , Lei GENG , Zhenhua LV , Longli LI
- 申请人: Shandong Dazhan Nano Materials Co., LTD , Ganhai Semiconductor Materials (Shanghai) Co., LTD.
- 申请人地址: CN Binzhou
- 专利权人: Shandong Dazhan Nano Materials Co., LTD,Ganhai Semiconductor Materials (Shanghai) Co., LTD.
- 当前专利权人: Shandong Dazhan Nano Materials Co., LTD,Ganhai Semiconductor Materials (Shanghai) Co., LTD.
- 当前专利权人地址: CN Binzhou
- 优先权: CN 2010066798.5 2020.01.20
- 国际申请: PCT/CN2020/134160 2020.12.07
- 进入国家日期: 2023-07-07
- 主分类号: C01B32/164
- IPC分类号: C01B32/164 ; C01B32/162 ; C01B3/26 ; B01J8/02 ; B01J8/00
摘要:
A method of continuously producing carbon nanotubes and hydrogencomprising: preparing a catalyst precursor, and pre-reducing the catalyst precursor; adding a height of carbon nanotubes in a reactor as a stacked bed and electrically heating the carbon nanotubes to the reaction temperature of a vapor deposition furnace in the presence of a protective gas; putting the pre-reduced catalyst or unreduced catalyst precursor into the reactor; under the condition of stirring the solid materials in the reactor, introducing a carbon source gas, reacting same by means of the vapor deposition furnace to generate new carbon nanotubes and hydrogen, continuously discharging a part of carbon nanotubes and a part of hydrogen, and repeating these steps to achieve the continuous preparation of carbon nanotubes. The device has a high utilization rate of raw materials, can manufacture a large batch of carbon nanotubes with a high purity at one time, and is suitable for large-scale industrial production.
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