发明申请
US20050085536A1 Process for the preparation of 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane
有权
1-氢过氧基-16-氧杂二环[10.4.0]十六烷的制备方法
![Process for the preparation of 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane](/docs/US/2005-04-21/US20050085536A1/abs.jpg.600x600.jpg)
- 专利标题： Process for the preparation of 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane
- 专利标题（中）： 1-氢过氧基-16-氧杂二环[10.4.0]十六烷的制备方法
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申请号： US10939012申请日： 2004-09-10
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公开(公告)号： US20050085536A1公开(公告)日： 2005-04-21
- 发明人: Stefan Lambrecht , Werner Marks , Hans-Juergen Topp , Norbert Richter , Walter Kuhn
- 申请人： Stefan Lambrecht , Werner Marks , Hans-Juergen Topp , Norbert Richter , Walter Kuhn
- 优先权： DE10348168.0 20031016
- 主分类号： C07D311/94
- IPC分类号： C07D311/94 ; C07D315/00 ; C07D301/12
![Process for the preparation of 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane](/abs-image/US/2005/04/21/US20050085536A1/abs.jpg.150x150.jpg)
摘要：
Process for the preparation of 1-hydroperoxy-16-oxabicyclo[10.4.0]hexadecane (DDP-OOH), wherein 13-oxabicyclo[10.4.0]hexadec-1(12)-ene (DDP) and hydrogen peroxide are reacted in a diluent in the presence of a strong acid, the diluent has a pKa value of greater than or equal to 4.5 and the strong acid has a pKa value of less than or equal to 1.5, wherein after the reaction has taken place, the strong acid is neutralized with at least 0.9 molar equivalent of a base.
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