• Patent Title: Energy efficient biodiesel production from natural or industrial waste oil
  • Application No.: US17917514
    Application Date: 2021-03-30
  • Publication No.: US12031107B2
    Publication Date: 2024-07-09
  • Inventor: Paul KlingelhoeferMichael Schier
  • Applicant: BASF SE
  • Applicant Address: DE Ludwigshafen
  • Assignee: BASF SE
  • Current Assignee: BASF SE
  • Current Assignee Address: DE Ludwigshafen
  • Agency: ArentFox Schiff LLP
  • Priority: EP 168384 2020.04.07
  • International Application: PCT/EP2021/058362 2021.03.30
  • International Announcement: WO2021/204610A 2021.10.14
  • Date entered country: 2022-10-06
  • Main IPC: C11C3/02
  • IPC: C11C3/02 C10L1/02 C11C3/10
Energy efficient biodiesel production from natural or industrial waste oil
Abstract:
A method of producing fatty acid alkyl ester from an organic oil source containing at least one free fatty acid, wherein the vegetable and/or animal waste oil has an acid number of at least 30 mg KOH/g and wherein the method comprises the steps of a) reacting the oil source with glycerol at a temperature, which is at least 110° C. and does not exceed 180° C. during the reaction, in the presence of a catalyst comprising at least methane sulfonic acid or the homo anhydride thereof; and b) acidic transesterification at a temperature, which is at least 110° C. and does not exceed 160° C. during the reaction of the reaction product from step a) with an alkanol; and c) isolating the fatty acid alkyl ester from the reaction product of step b).
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