- 专利标题: Method for producing phosphoric acid and by-producing alpha-hemihydrate gypsum by wet-process
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申请号: US15760851申请日: 2016-08-26
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公开(公告)号: US10745278B2公开(公告)日: 2020-08-18
- 发明人: Zhaoping Hu , Hongkun Chen , Hualong Yao , Yongxiu Liu , Chengzhi Li , Xixing Zhang
- 申请人: KINGENTA ECOLOGICAL ENGINEERING GROUP CO., LTD. , KINGENTA NORSTERRA CHEMICAL CO., LTD.
- 申请人地址: CN Shandong CN Guizhou
- 专利权人: Kingenta Ecological Engineering Group Co., Ltd.,Kingenta Norsterra Chemical Co., Ltd.
- 当前专利权人: Kingenta Ecological Engineering Group Co., Ltd.,Kingenta Norsterra Chemical Co., Ltd.
- 当前专利权人地址: CN Shandong CN Guizhou
- 代理机构: RatnerPrestia
- 优先权: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@19a42e09
- 国际申请: PCT/CN2016/096941 WO 20160826
- 国际公布: WO2017/045520 WO 20170323
- 主分类号: C01B25/229
- IPC分类号: C01B25/229 ; C01F11/46 ; C01B25/22
摘要:
Provided is a method for producing phosphoric acid and at the same time obtaining alpha-hemihydrate gypsum including: adding a phosphate rock powder and a part of dilute sulfuric acid into an extraction tank, carrying out an extraction reaction on same, separating a clear liquid from the obtained mixed slurry, sending the clear liquid, as a finished product phosphoric acid, into an acid storeroom, and transferring a separated solid, together with the rest mixed slurry, into a crystal transformation tank; and adding sulfuric acid and a crystal transformation agent into the crystal transformation tank, carrying out a crystal transformation reaction for 1.5-7.5 h at 60° C.-130° C., and solid-liquid separating the obtained mixed acid slurry, wherein the solid can be dried into a gypsum powder, or may be not subjected to a drying step and made into gypsum products such as gypsum boards, gypsum building blocks and gypsum members by directly adding water.
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