- 专利标题: Process for preparing a titanium-containing zeolitic material having an MWW framework structure
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申请号: US14764354申请日: 2014-02-05
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公开(公告)号: US10029244B2公开(公告)日: 2018-07-24
- 发明人: Andrei-Nicolae Parvulescu , Ulrich Mueller , Hans-Juergen Luetzel , Georg Uhl , Robert Bayer , Regina Vogelsang , Joaquim Henrique Teles , Dominic Riedel , Daniel Urbanczyk , Ulrike Wegerle
- 申请人: BASF SE
- 申请人地址: DE Ludwigshafen
- 专利权人: BASF SE
- 当前专利权人: BASF SE
- 当前专利权人地址: DE Ludwigshafen
- 代理机构: Oblon, McClelland, Maier & Neustadt, L.L.P.
- 优先权: EP13154021 20130205
- 国际申请: PCT/EP2014/052205 WO 20140205
- 国际公布: WO2014/122152 WO 20140814
- 主分类号: C01B39/48
- IPC分类号: C01B39/48 ; B01J29/89 ; B01J37/00 ; B01J29/70 ; C01B39/08
摘要:
A process for the preparation of a titanium-containing zeolitic material having an MWW framework structure, the process comprising (i) providing a zeolitic material having an MWW framework structure comprising SiO2 and B2O3, (ii) incorporating titanium into the zeolitic material provided in (i) comprising (ii.I) preparing an aqueous synthesis mixture containing the zeolitic material provided in (i), an MWW template compound and a titanium source, (ii.2) hydrothermally synthesizing a titanium-containing zeolitic material having an MWW framework structure from the aqueous synthesis mixture prepared in (ii.1), obtaining a mother liquor comprising the titanium-containing zeolitic material having an MWW framework structure; (iii) spray-drying the mother liquor obtained from (ii.2) comprising the titanium-containing zeolitic material having an MWW framework structure.
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