The invention relates to the field of preparation of MOFs materials, and specifically relates to a method for rapid synthesis of MOFs materials with a molecular sieve for solvent recovery. According to the invention, a mechanism of solvent recovery by a molecular sieve is introduced during synthesis, so that reactant concentration in a solution can be constantly maintained at a relatively high level; with evaporation of a solvent into the molecular sieve, reactants crystallize quickly to be separated out, thereby accelerating the reaction; and a relatively dry product can be obtained when the solvent evaporates completely with no need for filtering and washing steps. In addition, the inventors introduce the way of holding the solvent in the molecular sieve to absolutely ensure that the solvent evaporates from the molecular sieve during reaction, and the solvent after the completion of the reaction is completely recovered into the molecular sieve; and moreover, a treatment process resulting from condensation of the solvent into the reactants during cooling after the completion of the reaction is avoided, so that the relatively dry product is obtained, and the filtering and washing steps are avoided.