The invention relates to a Hangjin 2# soil loaded nano-zero valent iron adsorption material, wherein the mass ratio of nano-zero valent iron to Hangjin 2# soil is 1:4-5. The preparation method employs Hangjin 2# soil as the carrier to load nano-zero valent iron, and the steps include: 1) dissolving an iron-containing oxide in an ethanol solution to obtain a mixed solution; 2) adding Hangjin 2# soil into the mixed solution of step 1, and controlling the mass ratio of nano-zero valent iron to Hangjin 2# soil at 1:4-5; 3) introducing nitrogen into the product of step 2, conducting stirring to remove oxygen; 4) adding a reducing agent into the product of step 3 to reduce the iron-containing oxide into nano-zero valent iron, and uniformly dispersing the nano-zero valent iron on the surface of the carrier material Hangjin 2# soil; and 5) subjecting the product obtained in step 4 to solid-liquid separation, and performing vacuum drying on the solid, thus obtaining the Hangjin 2# soil loaded nano-zero valent iron adsorption material. The adsorption material provided by the invention has higher reaction activity and reduction effectiveness, and has good application value in actual water pollution control and restoration projects.